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Proton, Electron, and Hydrogen-Atom Transfer Thermodynamics of the Metal–Organic Framework, Ti-MIL-125, Are Intrinsically Correlated to the Structural Disorder

Journal of the American Chemical Society Nazmiye Gökçe Altınçekiç, Chance W. Lander, Jiaqi Yu et al. Sep 24, 2025 DOI: 10.1021/jacs.5c10498

Burden and characteristics of inherited retinal diseases in China

Scientific Reports Yuqing Lin, Xiyang Dou, Lihong Li et al. Sep 24, 2025 DOI: 10.1038/s41598-025-17714-7

It’s not wokeness — it’s human rights

Nature Lesley Evans Ogden Sep 24, 2025 DOI: 10.1038/d41586-025-02932-w

Catalytic Consequences of Pore Structure, Nodal Identity, and Coordination Environment on Styrene Oxidation by Hydrogen Peroxide over Fe MOFs

Journal of the American Chemical Society Rachel A. Yang, James L. Trettin, Joshua L. Miller et al. Sep 24, 2025 DOI: 10.1021/jacs.5c08736

Exploring associations between sleep duration and performance as well as heart rate variability in elite esports athletes

Scientific Reports Peter Hoang, Mark Deppe, Brenden Alvarez et al. Sep 24, 2025 DOI: 10.1038/s41598-025-18228-y

Abstract Sleep is essential for overall well-being, influencing physical, psychological, and mental health. While research shows that increasing sleep enhances athletic performance, data on the relationship between performance, sleep, and stress response in esports athletes remains limited. Our study aims to explore sleep counseling and its associations on neurocognitive function, gaming performance, and heart rate variability in esports. We enrolled competitive Valorant esports athletes. Participants maintained their regular sleep schedule for four to six weeks, followed by an attempted four-week sleep extension phase. Health data were collected via a wearable device. We evaluated individual performance through neurocognitive tests and by analyzing participants’ weekly match statistics. The study revealed that participants did not significantly increase sleep duration (p = 0.265). We observed improvements in neurocognitive test reaction times (p < 0.01) but not gaming performance. Sleep counseling was also associated with improved heart rate variability (p < 0.05), though the effect size was small. Overall, this study highlights the difficulty of implementing behavioral sleep interventions in elite esports athletes and the need for alternative or more targeted approaches. While the intervention did not achieve significant sleep extension and therefore constrained causal inference, the study demonstrates the feasibility of a rigorous methodological framework for investigating sleep and performance in esports athletes.

Isotropic Zero Thermal Expansion in Yb(Al,Mn)<sub>2</sub>: Achieving Continuous Shiftability over a Wide Temperature Range

Journal of the American Chemical Society Hao Wang, Yuanji Xu, Yuzhu Song et al. Sep 24, 2025 DOI: 10.1021/jacs.5c10024

Machine learning model optimization for flood susceptibility zonation over the Kosi megafan, Himalayan foreland basin, India

Scientific Reports Aman Arora, Purna Durga G, Manish Pandey et al. Sep 24, 2025 DOI: 10.1038/s41598-025-07403-w

Macromolecular Diamidobenzimidazole Conjugates Can Activate Stimulator of Interferon Genes

Journal of the American Chemical Society Karan Arora, Taylor L. Sheehy, Jacob A. Schulman et al. Sep 24, 2025 DOI: 10.1021/jacs.5c13195

In transfusion-dependent thalassemia, neuronal damage biomarkers are associated with affective and chronic fatigue symptoms

Scientific Reports Maha Abdul Saheb Ridhaa, Hussein Kadhem Al-Hakeim, Mohammed K. Kahlol et al. Sep 24, 2025 DOI: 10.1038/s41598-025-16757-0

Arousal reframed as an organism‑wide dynamic system

Nature Sep 24, 2025 DOI: 10.1038/d41586-025-03067-8

The Divergent Reduction Chemistry of Ln(II) Bis(terphenylthiolate) Complexes, Ln(SAr<sup><i>i</i>Pr6</sup>)<sub>2</sub>, Leads to KLn(μ-SAr<sup><i>i</i>Pr6</sup>)<sub>2</sub>, C─H Bond Activation Products, and Two-Electron Reduction Reactivity

Journal of the American Chemical Society Makayla R. Luevano, Cary R. Stennett, Eric Ma et al. Sep 24, 2025 DOI: 10.1021/jacs.5c14054

Diesel particulate matter-induced proteomic changes in three-dimensional spheroids derived from human primary cells of various tissue origins

Scientific Reports Yoon Jin Cho, Hae Dong Jeong, Young June Jeon et al. Sep 24, 2025 DOI: 10.1038/s41598-025-17873-7

Abstract This study investigated the effects of diesel particulate matter (DPM) on multiple human organs using 3D spheroids derived from eight human primary cell types. To assess the impact of DPM, we exposed these spheroids to varying concentrations of standardized DPM (Standard Reference Material, SRM 2975) and measured their viability, followed by proteomic analysis using tandem mass tag (TMT) labeling with liquid chromatography–tandem mass spectrometry (LC-MS/MS). A total of 9,707 proteins were identified, with 128 proteins exhibiting statistically significant changes (P-value &lt; 0.05) in response to DPM exposure, as determined by two-way analysis of variance (ANOVA). Among these, five proteins, including apolipoprotein A-I (APOA1), significantly increased at higher DPM concentrations, while 36 proteins, primarily ribosomal proteins, showed notable decreases even at lower DPM levels. Canonical pathway analysis revealed activation of acute phase response signaling, liver X receptor/retinoid X receptor (LXR/RXR), and farnesoid X receptor (FXR)/RXR pathways across all spheroid types. APOA1 was identified as a potential biomarker for DPM exposure, with increased expression potentially linked to disruption in protein degradation pathways. This study provides valuable insights into the systemic toxicity of DPM, highlighting key proteomic changes across different tissue types and identifying potential biomarkers that could be used to assess exposure levels and health risks related to particulate matter.

Optimizing the Synthesis of Deuterated Isotopomers and Isotopologues of Cyclohexene using Molecular Rotational Resonance Spectroscopy

Journal of the American Chemical Society Justin T. Weatherford-Pratt, Jacob A. Smith, Martin S. Holdren et al. Sep 24, 2025 DOI: 10.1021/jacs.5c12001

Integrated kinetic, thermodynamic, and statistical investigation of aniline blue dye removal using magnesium silicate nanoparticles

Scientific Reports Ahmed Magdy, Magdi E. A. Zaki, Maysa R. Mostafa et al. Sep 24, 2025 DOI: 10.1038/s41598-025-18726-z

Abstract Magnesium silicate nanoparticles were found to be an effective adsorbent for aniline blue dye from wastewater. Using the sol-gel technique, magnesium silicate nanoparticles were synthesized and characterized using X-ray diffraction (XRD), transmission electron microscope (TEM), Brunauer-Emmett-Teller (BET) surface area, and fourier transform infrared spectroscopy (FTIR). Aniline blue removal was done at room temperature, pH 4, and a dosage of 3 g/L was about 99% in the first 30 min. Magnesium silicate can also be used for four cycles to adsorb Aniline blue dye without the need for disposal, which supports the principle of recycling. Response surface methodology was used for statistical analysis to investigate the impact of the factors. By studying the isotherms, kinetics, and thermodynamics, it became clear that the adsorption process involves a physical interaction that adheres to the Freundlich isotherm, follows pseudo-first-order kinetics, with the boundary layer (film) diffusion identified as the rate-determining step. The process is endothermic and spontaneous. Magnesium silicate nanoparticles were successfully used to remove dye contaminants from various actual water samples. The material’s reliability and potential for real-world environmental applications were demonstrated by the high efficiency and consistent adsorption results across multiple sample types.

pH-Responsive Self-Assembly of Renal-Clearable Nanoparticles in the Kidneys: One Assembly per Endosome

Journal of the American Chemical Society Yingyu Huang, Jie Zheng, Mengxiao Yu Sep 24, 2025 DOI: 10.1021/jacs.5c10759

Searching for effective preprocessing method and CNN based architecture with efficient channel attention on speech emotion recognition

Scientific Reports Byunggun Kim, Younghun Kwon Sep 24, 2025 DOI: 10.1038/s41598-025-19887-7

Abstract Recently, Speech emotion recognition (SER) performance has steadily increased as multiple deep learning architectures have adapted. Especially, convolutional neural network (CNN) models with spectrogram data preprocessing are the most popular approach in the SER. However, designing an effective and efficient preprocessing method and a CNN-based model for SER is still ambiguous. Therefore, it needs to search for more concrete preprocessing methods and a CNN-based model for SER. First, to search for a proper frequency-time resolution for SER, we prepare eight different datasets with preprocessing settings. Furthermore, to compensate for the lack of emotional feature resolution, we propose multiple short-term Fourier transform (STFT) preprocessing data augmentation that augments trainable data with all different sizes of windows. Next, because CNN’s channel filters are core to detecting hidden input features, we focus on the channel filters’ effectiveness on SER. To do so, we design several types of architecture that contain a 6-layer CNN model. Also, with efficient channel attention (ECA) that is well known to improve channel feature representation with only a few parameters, we find that it can more efficiently train the channel filters for SER. With two different SER datasets (Interactive Emotional Dyadic Motion Capture, Berlin Emotional Speech Database), increasing the frequency resolution in preprocessing emotional speech can improve emotion recognition performance. Consequently, the CNN-based model with only two ECA blocks can exceed the performance of previous SER models. Especially, with STFT data augmentation, our proposed model achieves the highest performance on SER.

Enzyme-Activated Sugar-Coated Bifunctional Degraders

Journal of the American Chemical Society Qian Zhu, Gerhard Fischer, Steven S. Cheng et al. Sep 24, 2025 DOI: 10.1021/jacs.5c09843

The long-term neuroprotective effect of MIND and Mediterranean diet on patients with Alzheimer’s disease

Scientific Reports Xiaofang Liu, Bo Yang, Qiong Liu et al. Sep 24, 2025 DOI: 10.1038/s41598-025-17055-5

Immunoglobulin-Directed Phase Separation for Cell-Specific Modulation of Receptor Signaling

Journal of the American Chemical Society Weishuai Ren, Peiyuan Zheng, Ziting Zhou et al. Sep 24, 2025 DOI: 10.1021/jacs.5c09699

Active vision-based real-time aquaculture net pens inspection using ROV

Scientific Reports Waseem Akram, Muhayy Ud Din, Mohamed Heshmat et al. Sep 24, 2025 DOI: 10.1038/s41598-025-21083-6