Nondestructive structural evaluation of high-aspect-ratio-etched holes by tender x-ray ptychography with computed tomography

N Naru Okawa (International Center for Synchrotron Radiation Innovation Smart, Tohoku University) N Nozomu Ishiguro (RIKEN SPring-8 Center, 1-1-1, Koto, Sayo, Hyogo 679-5148, Japan) Y Yuhei Sasaki (International Center for Synchrotron Radiation Innovation Smart, Tohoku University) M Masaki Abe (RIKEN SPring-8 Center, 1-1-1, Koto, Sayo, Hyogo 679-5148, Japan) S Shuntaro Takazawa (International Center for Synchrotron Radiation Innovation Smart, Tohoku University) M Mihiro Ikenaga Y Yukio Takahashi (RIKEN SPring-8 Center, 1-1-1, Koto, Sayo, Hyogo 679-5148, Japan)

Abstract

Nondestructive evaluation of high-aspect-ratio (HAR) structures in advanced memory devices is essential yet remains challenging at the nanoscale. In this study, we demonstrate tender x-ray ptychography for the characterization of HAR-etched hole structures with depths of approximately 10 μm. Reconstructed two-dimensional projection images, with a spatial resolution of 38.5 nm, reveal features such as necking at the amorphous carbon mask and tapered hole profiles. Furthermore, a three-dimensional (3D) electron density map was reconstructed using ptychographic x-ray computed tomography, achieving a spatial resolution of 67.5 nm. This approach enables direct visualization of etch-rate variations associated with aspect-ratio-dependent etching. These results establish a powerful nondestructive methodology for three-dimensional nanoscale evaluation of HAR structures, with significant potential for applications in advanced memory device development.

Article Details

Volume / Issue Vol. 129, Issue 1
Published July 06, 2026
ISSN 0003-6951
Publisher American Institute of Physics

Journal Info

Applied Physics Letters

American Institute of Physics

ISSN: 0003-6951 Physical Sciences

Authors (7)

N

Naru Okawa

International Center for Synchrotron Radiation Innovation Smart, Tohoku University

N

Nozomu Ishiguro

RIKEN SPring-8 Center, 1-1-1, Koto, Sayo, Hyogo 679-5148, Japan

Y

Yuhei Sasaki

International Center for Synchrotron Radiation Innovation Smart, Tohoku University

M

Masaki Abe

RIKEN SPring-8 Center, 1-1-1, Koto, Sayo, Hyogo 679-5148, Japan

S

Shuntaro Takazawa

International Center for Synchrotron Radiation Innovation Smart, Tohoku University

M

Mihiro Ikenaga

Y

Yukio Takahashi

RIKEN SPring-8 Center, 1-1-1, Koto, Sayo, Hyogo 679-5148, Japan