Mo-doped Ni/NiO supported on oxygen-deficient NiMoO4 with carbon derived from tannic acid for hydrogen evolution and hydrogen oxidation

X Xueqi Chen L Lijie Zhu (State Key Laboratory of Natural Medicines and Jiangsu Key Laboratory of Bioactive Natural Product Research, School of Traditional Chinese Pharmacy) H Hongzhan Chen (Siyuan Laboratory, Guangzhou Key Laboratory of Vacuum Coating Technologies and New Energy Materials, Guangdong Provincial Engineering Technology Research Center of Vacuum Coating Technologies and New Energy Materials, Guangdong Provincial Key Laboratory of Nanophotonic Manipulation, Department of Physics, Jinan University 1 , Guangzhou, Guangdong 510632,) Y Ya Tang F Feng Lin F Fangyan Xie (Instrumental Analysis and Research Center Sun Yat‐sen University Guangzhou 510275 China) J Jian Chen N Nan Wang Y Yanshuo Jin (Siyuan Laboratory, Guangzhou Key Laboratory of Vacuum Coating Technologies and New Energy Materials, Guangdong Provincial Engineering Technology Research Center of Vacuum Coating Technologies and New Energy Materials, Guangdong Provincial Key Laboratory of Nanophotonic Manipulation, Department of Physics, Jinan University 1 , Guangzhou, Guangdong 510632,) H Hui Meng (Department of Mechanical and Aerospace Engineering)

Abstract

The widespread deployment of anion exchange membrane unitized reversible fuel cells is contingent upon the development of stable and efficient non-precious metal electrocatalysts for the hydrogen oxidation reaction (HOR) and hydrogen evolution reaction (HER). This study reports on the synthesis of Mo-doped Ni/NiO hetero-nanoparticles supported on oxygen-deficient NiMoO4 (NiMoOX), with tannic acid (TA) integrated as both a carbon source and stabilizing agent (Ni/NiO-Mo/C@NiMoOX). In situ Raman spectroscopy elucidates the mechanism through which TA enhances the electrocatalytic activity. The resultant catalyst demonstrates superior HOR/HER performance, featuring a current density of 2.5 mA cm−2 at 100 mV overpotential for HOR, remaining stable for 24 h, and in HER, exhibiting a remarkably low overpotential of just −12 mV at a current density of −10 mA cm−2, with stability persisting for over 300 h, outperforming the commercial Pt/C catalyst.

Article Details

Volume / Issue Vol. 126, Issue 9
Published March 01, 2025
ISSN 0003-6951
Publisher American Institute of Physics

Journal Info

Applied Physics Letters

American Institute of Physics

ISSN: 0003-6951 Physical Sciences

Authors (10)

X

Xueqi Chen

L

Lijie Zhu

State Key Laboratory of Natural Medicines and Jiangsu Key Laboratory of Bioactive Natural Product Research, School of Traditional Chinese Pharmacy

H

Hongzhan Chen

Siyuan Laboratory, Guangzhou Key Laboratory of Vacuum Coating Technologies and New Energy Materials, Guangdong Provincial Engineering Technology Research Center of Vacuum Coating Technologies and New Energy Materials, Guangdong Provincial Key Laboratory of Nanophotonic Manipulation, Department of Physics, Jinan University 1 , Guangzhou, Guangdong 510632,

Y

Ya Tang

F

Feng Lin

F

Fangyan Xie

Instrumental Analysis and Research Center Sun Yat‐sen University Guangzhou 510275 China

J

Jian Chen

N

Nan Wang

Y

Yanshuo Jin

Siyuan Laboratory, Guangzhou Key Laboratory of Vacuum Coating Technologies and New Energy Materials, Guangdong Provincial Engineering Technology Research Center of Vacuum Coating Technologies and New Energy Materials, Guangdong Provincial Key Laboratory of Nanophotonic Manipulation, Department of Physics, Jinan University 1 , Guangzhou, Guangdong 510632,

H

Hui Meng

Department of Mechanical and Aerospace Engineering