Dark-field x-ray microscopy for 2D and 3D imaging of microstructural dynamics at the European x-ray free-electron laser

S Sara J. Irvine (Department of Applied Physics, Stanford University 1 , Stanford, California 94305,) K Kento Katagiri T Trygve M. Ræder (Department of Physics, Technical University of Denmark 5 , Kgs. Lyngby 2800,) U Ulrike Boesenberg (European X-Ray Free-Electron Laser Facility) D Darshan Chalise (SLAC National Accelerator Laboratory 2 , Menlo Park, California 94025,) J Jade I. Stanton (Department of Applied Physics, Stanford University 1 , Stanford, California 94305,) D Dayeeta Pal (SLAC National Accelerator Laboratory 2 , Menlo Park, California 94025,) J Jörg Hallmann (European X-Ray Free-Electron Laser Facility) G Gabriele Ansaldi (European X-Ray Free-Electron Laser Facility 6 , Schenefeld 22869,) F Felix Brausse (European X-Ray Free-Electron Laser Facility) J Jon H. Eggert L Lichao Fang (SLAC National Accelerator Laboratory 2 , Menlo Park, California 94025,) E Eric Folsom (Lawrence Livermore National Laboratory 7 , Livermore, California 94550,) M Morten Haubro (Department of Physics, Technical University of Denmark 5 , Kgs. Lyngby 2800,) T Theodor S. Holstad (Department of Physics, Technical University of Denmark 5 , Kgs. Lyngby 2800,) A Anders Madsen (European X-Ray Free-Electron Laser Facility) J Johannes Möller (European X-Ray Free-Electron Laser Facility) M Martin M. Nielsen H Henning F. Poulsen (Department of Physics, Technical University of Denmark 5 , Kgs. Lyngby 2800,) J Jan-Etienne Pudell (European X-Ray Free-Electron Laser Facility) A Angel Rodriguez-Fernandez (European X-Ray Free-Electron Laser Facility) F Frank Schoofs (FS Consulting 8 , Marlow,) F Frank Seiboth Y Yifan Wang W Wonhyuk Jo (European X-Ray Free-Electron Laser Facility) M Mohamed Youssef (European X-Ray Free-Electron Laser Facility) A Alexey Zozulya (European X-Ray Free-Electron Laser Facility) K Kristoffer Haldrup (Department of Physics, Technical University of Denmark 1 , DK-2800 Kgs. Lyngby,) L Leora E. Dresselhaus-Marais (SLAC National Accelerator Laboratory 2 , Menlo Park, California 94025,)

Abstract

Dark field x-ray microscopy (DXFM) can visualize microstructural distortions in bulk crystals. Using the femtosecond x-ray pulses generated by x-ray free-electron lasers (XFELs), DFXM can achieve sub-μm spatial resolution and <100 fs time resolution simultaneously. In this paper, we demonstrate ultrafast DFXM measurements at the European XFEL to visualize an optically driven longitudinal strain wave propagating through a diamond single crystal. We also present two DFXM scanning modalities that are new to the XFEL sources: spatial 3D and 2D axial-strain scans with sub-μm spatial resolution. With this progress in XFEL-based DFXM, we discuss new opportunities to study multi-timescale spatiotemporal dynamics of microstructures.

Article Details

Volume / Issue Vol. 137, Issue 5
Published February 07, 2025
ISSN 0021-8979
Publisher American Institute of Physics

Journal Info

Journal of Applied Physics

American Institute of Physics

ISSN: 0021-8979 Physical Sciences

Authors (29)

S

Sara J. Irvine

Department of Applied Physics, Stanford University 1 , Stanford, California 94305,

K

Kento Katagiri

T

Trygve M. Ræder

Department of Physics, Technical University of Denmark 5 , Kgs. Lyngby 2800,

U

Ulrike Boesenberg

European X-Ray Free-Electron Laser Facility

D

Darshan Chalise

SLAC National Accelerator Laboratory 2 , Menlo Park, California 94025,

J

Jade I. Stanton

Department of Applied Physics, Stanford University 1 , Stanford, California 94305,

D

Dayeeta Pal

SLAC National Accelerator Laboratory 2 , Menlo Park, California 94025,

J

Jörg Hallmann

European X-Ray Free-Electron Laser Facility

G

Gabriele Ansaldi

European X-Ray Free-Electron Laser Facility 6 , Schenefeld 22869,

F

Felix Brausse

European X-Ray Free-Electron Laser Facility

J

Jon H. Eggert

L

Lichao Fang

SLAC National Accelerator Laboratory 2 , Menlo Park, California 94025,

E

Eric Folsom

Lawrence Livermore National Laboratory 7 , Livermore, California 94550,

M

Morten Haubro

Department of Physics, Technical University of Denmark 5 , Kgs. Lyngby 2800,

T

Theodor S. Holstad

Department of Physics, Technical University of Denmark 5 , Kgs. Lyngby 2800,

A

Anders Madsen

European X-Ray Free-Electron Laser Facility

J

Johannes Möller

European X-Ray Free-Electron Laser Facility

M

Martin M. Nielsen

H

Henning F. Poulsen

Department of Physics, Technical University of Denmark 5 , Kgs. Lyngby 2800,

J

Jan-Etienne Pudell

European X-Ray Free-Electron Laser Facility

A

Angel Rodriguez-Fernandez

European X-Ray Free-Electron Laser Facility

F

Frank Schoofs

FS Consulting 8 , Marlow,

F

Frank Seiboth

Y

Yifan Wang

W

Wonhyuk Jo

European X-Ray Free-Electron Laser Facility

M

Mohamed Youssef

European X-Ray Free-Electron Laser Facility

A

Alexey Zozulya

European X-Ray Free-Electron Laser Facility

K

Kristoffer Haldrup

Department of Physics, Technical University of Denmark 1 , DK-2800 Kgs. Lyngby,

L

Leora E. Dresselhaus-Marais

SLAC National Accelerator Laboratory 2 , Menlo Park, California 94025,