Yb‐Doped Cu‐Based Catalyst Boosting Electrochemical CO <sub>2</sub> ‐to‐C <sub>2+</sub> Reduction Across pH Range at Ampere‐Level Current Density

A Ao Feng N Nan Fang X Xiao‐Tian Yuan (State Key Laboratory of Physical Chemistry of Solid Surface College of Chemistry and Chemical Engineering Xiamen University Xiamen 361005 China) K Kun‐Lin Li (State Key Laboratory of Physical Chemistry of Solid Surface College of Chemistry and Chemical Engineering Xiamen University Xiamen 361005 China) X Xuantao Deng (State Key Laboratory of Physical Chemistry of Solid Surface College of Chemistry and Chemical Engineering Xiamen University Xiamen 361005 China) J Jia‐Feng Du (State Key Laboratory of Physical Chemistry of Solid Surfaces College of Chemistry and Chemical Engineering Xiamen University Xiamen China) Z Zhi‐Ming Zhang (State Key Laboratory of Crystal Materials Institute for New Energy Materials and Low Carbon Technologies School of Materials Science and Engineering Tianjin University of Technology Tianjin China) S Si‐Ying Li (State Key Laboratory of Physical Chemistry of Solid Surface College of Chemistry and Chemical Engineering Xiamen University Xiamen 361005 China) D De‐Yin Wu (State Key Laboratory of Physical Chemistry of Solid Surface College of Chemistry and Chemical Engineering Xiamen University Xiamen 361005 China) J Jin‐Yu Ye (State Key Laboratory of Physical Chemistry of Solid Surfaces College of Chemistry and Chemical Engineering Xiamen University Xiamen China) Q Qi‐Zheng Zheng (Institute of New Energy Materials and Engineering College of Materials Science and Engineering Fujian Engineering Research Center of High Energy Batteries and New Energy Equipment &amp; Systems Fuzhou University Fuzhou 350108 China) Z Zhi‐You Zhou (State Key Laboratory of Physical Chemistry of Solid Surfaces College of Chemistry and Chemical Engineering Xiamen University Xiamen China) S Shi‐Gang Sun (State Key Laboratory of Physical Chemistry of Solid Surfaces College of Chemistry and Chemical Engineering Xiamen University Xiamen P. R. China)

Abstract

Abstract Efficient electrochemical conversion of CO 2 to multi‐carbon (C 2+ ) products remains significant challenges, particularly under broad pH ranges and high‐current‐density conditions. Herein, we report ampere‐level CO 2 ‐to‐C 2+ electroreduction with exceptional efficiency across a wide pH range using ytterbium‐doped CuO x catalysts. The catalyst achieves Faradaic efficiency of 87 ± 2%, 77 ± 1%, and 78 ± 1% under alkaline, neutral, and acidic conditions, respectively. Electrochemical in situ infrared spectroscopy and Raman spectroscopy reveal that Yb‐stabilizing Cu + species and enriching *CO on Cu terrace sites are two critical factors for enhancing C─C coupling. This work not only develops a highly efficient electrocatalysts for sustainable C 2+ production, but also establishes a doping strategy for stabilizing active sites and optimizing *CO adsorption configurations.

Article Details

Volume / Issue Vol. 65, Issue 8
Published February 16, 2026
ISSN 1433-7851
Publisher Wiley

Journal Info

Angewandte Chemie International Edition

Wiley

ISSN: 1433-7851 Physical Sciences

Authors (13)

A

Ao Feng

N

Nan Fang

X

Xiao‐Tian Yuan

State Key Laboratory of Physical Chemistry of Solid Surface College of Chemistry and Chemical Engineering Xiamen University Xiamen 361005 China

K

Kun‐Lin Li

State Key Laboratory of Physical Chemistry of Solid Surface College of Chemistry and Chemical Engineering Xiamen University Xiamen 361005 China

X

Xuantao Deng

State Key Laboratory of Physical Chemistry of Solid Surface College of Chemistry and Chemical Engineering Xiamen University Xiamen 361005 China

J

Jia‐Feng Du

State Key Laboratory of Physical Chemistry of Solid Surfaces College of Chemistry and Chemical Engineering Xiamen University Xiamen China

Z

Zhi‐Ming Zhang

State Key Laboratory of Crystal Materials Institute for New Energy Materials and Low Carbon Technologies School of Materials Science and Engineering Tianjin University of Technology Tianjin China

S

Si‐Ying Li

State Key Laboratory of Physical Chemistry of Solid Surface College of Chemistry and Chemical Engineering Xiamen University Xiamen 361005 China

D

De‐Yin Wu

State Key Laboratory of Physical Chemistry of Solid Surface College of Chemistry and Chemical Engineering Xiamen University Xiamen 361005 China

J

Jin‐Yu Ye

State Key Laboratory of Physical Chemistry of Solid Surfaces College of Chemistry and Chemical Engineering Xiamen University Xiamen China

Q

Qi‐Zheng Zheng

Institute of New Energy Materials and Engineering College of Materials Science and Engineering Fujian Engineering Research Center of High Energy Batteries and New Energy Equipment &amp; Systems Fuzhou University Fuzhou 350108 China

Z

Zhi‐You Zhou

State Key Laboratory of Physical Chemistry of Solid Surfaces College of Chemistry and Chemical Engineering Xiamen University Xiamen China

S

Shi‐Gang Sun

State Key Laboratory of Physical Chemistry of Solid Surfaces College of Chemistry and Chemical Engineering Xiamen University Xiamen P. R. China