Unlocking Durable and Sustainable Zinc–Iodine Batteries via Molecularly Engineered Polyiodide Reservoirs

L Leiqian Zhang (Key Laboratory of Synthetic and Biological Colloids Ministry of Education School of Chemical and Material Engineering Jiangnan University Wuxi 214122 P.R. China) K Ke Luo (State Key Laboratory of Chemo and Biosensing, College of Chemistry and Chemical Engineering) J Jiaming Gong (State Key Laboratory of Metal Matrix Composites School of Materials Science and Engineering Shanghai Jiao Tong University Shanghai 200240 P.R. China) Y Yazhou Zhou (Institute of Physics, Chinese Academy of Sciences) H Hele Guo (Key Laboratory of Synthetic and Biological Colloids, Ministry of Education, School of Chemical and Material Engineering, International Joint Research Laboratory for Nano Energy Composites) Y Yi Yu G Guanjie He (Christopher Ingold Laboratory, Department of Chemistry, University College London, 20 Gordon Street, London WC1H 0AJ, U.K.) J Jean‐François Gohy (Institute of Condensed Matter and Nanoscience (IMCN) Université catholique de Louvain Place L. Pasteur 1 Louvain‐la‐Neuve 1348 Belgium) I Ivan P. Parkin (Christopher Ingold Laboratory, Department of Chemistry, University College London, 20 Gordon Street, London WC1H 0AJ, U.K.) J Johan Hofkens (Department of Chemistry, KU Leuven, Celestijnenlaan 200F, B-3001 Leuven, Belgium) Q Qing He T Tianxi Liu (Key Laboratory of Synthetic and Biological Colloids, Ministry of Education, School of Chemical and Material Engineering) K Klaus Müllen F Feili Lai (Department of Chemistry, KU Leuven, Celestijnenlaan 200F, Leuven 3001, Belgium)

Abstract

Abstract Zinc–iodine batteries (ZIBs) are promising candidates for safe and sustainable energy storage but are hindered by polyiodide shuttling, leading to rapid capacity decay and limited cyclability. In this work, we propose a “polyiodide reservoirs” concept, utilizing iodophilic covalent organic cages to confine polyiodide through multiple noncovalent interactions. By precisely engineering the nitrogen‐active site densities around 3D cavities, these cages evolve from open to near‐enclosed structure, achieving molecular‐level polyiodide entrapment. The optimized superphane cage (18 N‐active sites) enables a ZIB with 90.1% capacity retention after 4000 cycles at 5 C, even under extreme conditions (58.9 wt% iodine content within the cage and an iodine area loading of 3.7 mg cm −2 in the cathode). Importantly, the cage's solubility‐driven regeneration capability retains 85.4% initial capacity over three reuse cycles. This work establishes covalent organic superphanes as a transformative platform for long‐life ZIBs, offering a dual solution to shuttle suppression and electrode sustainability through structural confinement and dynamic recyclability.

Article Details

Volume / Issue Vol. 64, Issue 30
Published July 21, 2025
ISSN 1433-7851
Publisher Wiley

Journal Info

Angewandte Chemie International Edition

Wiley

ISSN: 1433-7851 Physical Sciences

Authors (14)

L

Leiqian Zhang

Key Laboratory of Synthetic and Biological Colloids Ministry of Education School of Chemical and Material Engineering Jiangnan University Wuxi 214122 P.R. China

K

Ke Luo

State Key Laboratory of Chemo and Biosensing, College of Chemistry and Chemical Engineering

J

Jiaming Gong

State Key Laboratory of Metal Matrix Composites School of Materials Science and Engineering Shanghai Jiao Tong University Shanghai 200240 P.R. China

Y

Yazhou Zhou

Institute of Physics, Chinese Academy of Sciences

H

Hele Guo

Key Laboratory of Synthetic and Biological Colloids, Ministry of Education, School of Chemical and Material Engineering, International Joint Research Laboratory for Nano Energy Composites

Y

Yi Yu

G

Guanjie He

Christopher Ingold Laboratory, Department of Chemistry, University College London, 20 Gordon Street, London WC1H 0AJ, U.K.

J

Jean‐François Gohy

Institute of Condensed Matter and Nanoscience (IMCN) Université catholique de Louvain Place L. Pasteur 1 Louvain‐la‐Neuve 1348 Belgium

I

Ivan P. Parkin

Christopher Ingold Laboratory, Department of Chemistry, University College London, 20 Gordon Street, London WC1H 0AJ, U.K.

J

Johan Hofkens

Department of Chemistry, KU Leuven, Celestijnenlaan 200F, B-3001 Leuven, Belgium

Q

Qing He

T

Tianxi Liu

Key Laboratory of Synthetic and Biological Colloids, Ministry of Education, School of Chemical and Material Engineering

K

Klaus Müllen

F

Feili Lai

Department of Chemistry, KU Leuven, Celestijnenlaan 200F, Leuven 3001, Belgium