The XPS of pyridine: A combined theoretical and experimental analysis

P Paul S. Bagus (Department of Chemistry, University of North Texas 1 , Denton, Texas 76203-5017,) C Connie J. Nelin (Consultant 2 , Austin, Texas 78730,) M Michel Sassi (Physical and Computational Sciences Directorate and Institute for Integrated Catalysis, Pacific Northwest National Laboratory 3 , Richland, Washington 99352,) D Daniel Baranowski (Physical and Computational Sciences Directorate and Institute for Integrated Catalysis, Pacific Northwest National Laboratory 3 , Richland, Washington 99352,) M Marcus A. Sharp (Physical and Computational Sciences Directorate and Institute for Integrated Catalysis, Pacific Northwest National Laboratory 1 , Richland, Washington 99352,) T Tom Autrey (Physical and Computational Sciences Directorate and Institute for Integrated Catalysis, Pacific Northwest National Laboratory 3 , Richland, Washington 99352,) Z Zdenek Dohnálek (Physical and Computational Sciences Directorate and Institute for Integrated Catalysis, Pacific Northwest National Laboratory 3 , Richland, Washington 99352,) Z Zbynek Novotny (Physical and Computational Sciences Directorate and Institute for Integrated Catalysis, Pacific Northwest National Laboratory 3 , Richland, Washington 99352,)

Abstract

A detailed analysis of the N(1s) and C(1s) X-Ray Photoelectron Spectroscopy (XPS) is made, where the measured XPS is compared with theoretical Sudden Approximation (SA) intensities and theoretical XPS Binding Energies (BEs). There is remarkably good agreement between the theoretical predictions and the measured XPS; in particular, the different full width at half maximum values for the C(1s) and N(1s) BEs are explained in terms of unresolved C(1s) BEs for the different C atoms in pyridine. This work demonstrates that the combination of theory and XPS measurements can extract analysis of the XPS relevant to the molecular electronic structure. The theory used is based on fully relativistic self-consistent field solutions of the Dirac–Coulomb Hamiltonian, and the SA is used to determine relative XPS intensities.

Article Details

Volume / Issue Vol. 162, Issue 8
Published February 28, 2025
ISSN 0021-9606
Publisher American Institute of Physics

Journal Info

The Journal of Chemical Physics

American Institute of Physics

ISSN: 0021-9606 Physical Sciences

Authors (8)

P

Paul S. Bagus

Department of Chemistry, University of North Texas 1 , Denton, Texas 76203-5017,

C

Connie J. Nelin

Consultant 2 , Austin, Texas 78730,

M

Michel Sassi

Physical and Computational Sciences Directorate and Institute for Integrated Catalysis, Pacific Northwest National Laboratory 3 , Richland, Washington 99352,

D

Daniel Baranowski

Physical and Computational Sciences Directorate and Institute for Integrated Catalysis, Pacific Northwest National Laboratory 3 , Richland, Washington 99352,

M

Marcus A. Sharp

Physical and Computational Sciences Directorate and Institute for Integrated Catalysis, Pacific Northwest National Laboratory 1 , Richland, Washington 99352,

T

Tom Autrey

Physical and Computational Sciences Directorate and Institute for Integrated Catalysis, Pacific Northwest National Laboratory 3 , Richland, Washington 99352,

Z

Zdenek Dohnálek

Physical and Computational Sciences Directorate and Institute for Integrated Catalysis, Pacific Northwest National Laboratory 3 , Richland, Washington 99352,

Z

Zbynek Novotny

Physical and Computational Sciences Directorate and Institute for Integrated Catalysis, Pacific Northwest National Laboratory 3 , Richland, Washington 99352,