Suppressed Concentration Quenching Via Divalent Eu/Sr Alloying in Hybrid Iodides Scintillators Toward Bright Luminescence for X‐ray Imaging

L Lihan Chen (College of Computer and Data Science) S Shuai Zhang Y Yuzhen Wang (State Key Laboratory of Luminescent Materials and Devices, Guangdong Provincial Key Laboratory of Fiber Laser Materials and Applied Techniques, School of Physics and Optoelectronics) L Liang Li D Dongdan Chen (State Key Laboratory of Luminescent Materials and Devices Guangdong Provincial Key Laboratory of Fiber Laser Materials and Applied Techniques School of Materials Science and Engineering South China University of Technology Guangzhou 510641 China) K Kai Han (Key Laboratory of Medical Molecule Science and Pharmaceutics Engineering, Ministry of Industry and Information Technology, School of Chemistry and Chemical Engineering, Center for Quantum Technology Research and School of Physics) Z Zhiguo Xia (State Key Laboratory of Luminescent Materials and Devices, Guangdong Provincial Key Laboratory of Fiber Laser Materials and Applied Techniques, School of Physics and Optoelectronics)

Abstract

Abstract Overcoming concentration quenching in rare‐earth‐activated luminescent materials always remains a challenge for enhancing photoluminescence quantum yield (PLQY). Herein, we report two divalent Sr‐based hybrid iodides, (Ph 3 MeP)SrI 3 and (Ph 3 EtP)SrI 3 (Ph 3 MeP = methyltriphenylphosphonium, Ph 3 EtP = ethyltriphenylphosphonium), and equivalent Eu/Sr alloying have been identified experimentally in the full range of 0 ≤  x  ≤ 1 for (Ph 3 MeP)Sr (1‐ x ) Eu x I 3 and (Ph 3 EtP)Sr (1‐ x ) Eu x I 3 . These Eu/Sr‐based hybrid iodides exhibit 1D [Sr (1‐ x ) Eu x I 6 ] 4− octahedra chains, suppressing nonradiative energy loss effectively by maintaining optimal spacing and dispersion between adjacent Eu(II) emission centers. Upon even heavily Eu(II) alloying, (Ph 3 MeP)Sr 0.5 Eu 0.5 I 3 exhibits efficient green emission ( λ em = 525 nm) with a high PLQY of ∼92.2%. Accordingly, it achieves a high scintillation light yield of 54 000 ± 300 ph MeV −1 and a low detection limit of 49.9 nGy s −1 . Furthermore, ceramic wafers counterparts of Eu/Sr alloy prepared via cold sintering process demonstrate high‐resolution X‐ray imaging with a spatial resolution up to 15.7 lp mm −1 . These findings not only present a new family of hybrid bimetallic iodides via Eu/Sr alloying, but also provides structurally guided strategy to suppress concentration quenching toward bright luminescence for scintillation applications.

Article Details

Volume / Issue Vol. 64, Issue 49
Published December 01, 2025
ISSN 1433-7851
Publisher Wiley

Journal Info

Angewandte Chemie International Edition

Wiley

ISSN: 1433-7851 Physical Sciences

Authors (7)

L

Lihan Chen

College of Computer and Data Science

S

Shuai Zhang

Y

Yuzhen Wang

State Key Laboratory of Luminescent Materials and Devices, Guangdong Provincial Key Laboratory of Fiber Laser Materials and Applied Techniques, School of Physics and Optoelectronics

L

Liang Li

D

Dongdan Chen

State Key Laboratory of Luminescent Materials and Devices Guangdong Provincial Key Laboratory of Fiber Laser Materials and Applied Techniques School of Materials Science and Engineering South China University of Technology Guangzhou 510641 China

K

Kai Han

Key Laboratory of Medical Molecule Science and Pharmaceutics Engineering, Ministry of Industry and Information Technology, School of Chemistry and Chemical Engineering, Center for Quantum Technology Research and School of Physics

Z

Zhiguo Xia

State Key Laboratory of Luminescent Materials and Devices, Guangdong Provincial Key Laboratory of Fiber Laser Materials and Applied Techniques, School of Physics and Optoelectronics