Superstrong Lightweight Aerogel with Supercontinuous Layer by Surface Reaction

T Tianpei Zhou (Key Laboratory of Precision and Intelligent Chemistry CAS Key Laboratory of Mechanical Behavior and Design of Materials Department of Precision Machinery and Precision Instrumentation National Synchrotron Radiation Laboratory Center for Micro and Nanoscale Research and Fabrication Institute of Advanced Technology University of Science and Technology of China Hefei 230026 P. R. China) L Linbo He (Key Laboratory of Precision and Intelligent Chemistry CAS Key Laboratory of Mechanical Behavior and Design of Materials Department of Precision Machinery and Precision Instrumentation National Synchrotron Radiation Laboratory Center for Micro and Nanoscale Research and Fabrication Institute of Advanced Technology University of Science and Technology of China Hefei 230026 P. R. China) Y Yu Zhen X Xiaolin Tai (State Key Laboratory of Precision and Intelligent Chemistry, School of Chemistry and Materials Science) S Shun Dai (Key Laboratory of Precision and Intelligent Chemistry CAS Key Laboratory of Mechanical Behavior and Design of Materials Department of Precision Machinery and Precision Instrumentation National Synchrotron Radiation Laboratory Center for Micro and Nanoscale Research and Fabrication Institute of Advanced Technology University of Science and Technology of China Hefei 230026 P. R. China) K Kaijin Wu H Honghe Ding (National Synchrotron Radiation Laboratory) T Tianpu Xia (Key Laboratory of Precision and Intelligent Chemistry CAS Key Laboratory of Mechanical Behavior and Design of Materials Department of Precision Machinery and Precision Instrumentation National Synchrotron Radiation Laboratory Center for Micro and Nanoscale Research and Fabrication Institute of Advanced Technology University of Science and Technology of China Hefei 230026 P. R. China) X Xun Zhang (Department of Chemistry, Graduate School of Science, The University of Tokyo, 7-3-1 Hongo, Bunkyo-ku, Tokyo 113-0033, Japan) X Xueru Cai (Key Laboratory of Precision and Intelligent Chemistry CAS Key Laboratory of Mechanical Behavior and Design of Materials Department of Precision Machinery and Precision Instrumentation National Synchrotron Radiation Laboratory Center for Micro and Nanoscale Research and Fabrication Institute of Advanced Technology University of Science and Technology of China Hefei 230026 P. R. China) F Fangzhou Jiang (Hefei National Laboratory for Physical Sciences at Microscale and Department of Physics) Z Zhiqiang Zhu (State Key Laboratory of Chemo and Biosensing, College of Chemistry and Chemical Engineering) F Fangsheng Huang (Key Laboratory of Precision and Intelligent Chemistry CAS Key Laboratory of Mechanical Behavior and Design of Materials Department of Precision Machinery and Precision Instrumentation National Synchrotron Radiation Laboratory Center for Micro and Nanoscale Research and Fabrication Institute of Advanced Technology University of Science and Technology of China Hefei 230026 P. R. China) C Chen Li (Sibley School of Mechanical and Aerospace Engineering, Cornell University, Ithaca, NY, USA.) Y Yaping Li (State Key Laboratory of Chemical Resource Engineering, College of Chemistry) J Junfa Zhu (National Synchrotron Radiation Laboratory) W Wangsheng Chu (National Synchrotron Radiation Laboratory) Y Yue Lin Y Yong Ni (CAS Key Laboratory of Mechanical Behavior and Design of Materials, Department of Modern Mechanics, CAS Center for Excellence in Complex System Mechanics) Y Yi Xie C Changzheng Wu (State Key Laboratory of Precision and Intelligent Chemistry, School of Chemistry and Materials Science)

Abstract

AbstractBreaking the thermal, mechanical and lightweight performance limit of aerogels has pivotal significance on thermal protection, new energy utilization, high‐temperature catalysis, structural engineering, and physics, but is severely limited by the serious discrete characteristics between grain boundary and nano‐units interfaces. Herein, a thermodynamically driven surface reaction and confined crystallization process is reported to synthesize a centimeter‐scale supercontinuous ZrO2 nanolayer on ZrO2‐SiO2 fiber aerogel surface, which significantly improved its thermal and mechanical properties with density almost unchanged (≈26 mg cm−3). Systematic structure analysis confirms that the supercontinuous layer achieves a close connection between grains and fibers through Zr─O─Si bonds. The as‐prepared aerogel exhibits record‐breaking specific strength (≈84615 N m kg−1, can support up to ≈227 272 times aerogel mass) and dynamic impact resistance (withstanding impacts up to 500 times aerogel mass and up to 200 cycling stability at 80% strain). Besides, its temperature resistance has also been greatly optimized (400 °C enhancement, stability at 1500 °C). This work will provide a new perspective for exploring the limits of lightweight, high strength, and thermal properties of solid materials.

Article Details

Volume / Issue Vol. 37, Issue 10
Published March 01, 2025
ISSN 0935-9648
Publisher Unknown Publisher

Journal Info

Advanced Materials

Unknown Publisher

ISSN: 0935-9648 Physical Sciences

Authors (21)

T

Tianpei Zhou

Key Laboratory of Precision and Intelligent Chemistry CAS Key Laboratory of Mechanical Behavior and Design of Materials Department of Precision Machinery and Precision Instrumentation National Synchrotron Radiation Laboratory Center for Micro and Nanoscale Research and Fabrication Institute of Advanced Technology University of Science and Technology of China Hefei 230026 P. R. China

L

Linbo He

Key Laboratory of Precision and Intelligent Chemistry CAS Key Laboratory of Mechanical Behavior and Design of Materials Department of Precision Machinery and Precision Instrumentation National Synchrotron Radiation Laboratory Center for Micro and Nanoscale Research and Fabrication Institute of Advanced Technology University of Science and Technology of China Hefei 230026 P. R. China

Y

Yu Zhen

X

Xiaolin Tai

State Key Laboratory of Precision and Intelligent Chemistry, School of Chemistry and Materials Science

S

Shun Dai

Key Laboratory of Precision and Intelligent Chemistry CAS Key Laboratory of Mechanical Behavior and Design of Materials Department of Precision Machinery and Precision Instrumentation National Synchrotron Radiation Laboratory Center for Micro and Nanoscale Research and Fabrication Institute of Advanced Technology University of Science and Technology of China Hefei 230026 P. R. China

K

Kaijin Wu

H

Honghe Ding

National Synchrotron Radiation Laboratory

T

Tianpu Xia

Key Laboratory of Precision and Intelligent Chemistry CAS Key Laboratory of Mechanical Behavior and Design of Materials Department of Precision Machinery and Precision Instrumentation National Synchrotron Radiation Laboratory Center for Micro and Nanoscale Research and Fabrication Institute of Advanced Technology University of Science and Technology of China Hefei 230026 P. R. China

X

Xun Zhang

Department of Chemistry, Graduate School of Science, The University of Tokyo, 7-3-1 Hongo, Bunkyo-ku, Tokyo 113-0033, Japan

X

Xueru Cai

Key Laboratory of Precision and Intelligent Chemistry CAS Key Laboratory of Mechanical Behavior and Design of Materials Department of Precision Machinery and Precision Instrumentation National Synchrotron Radiation Laboratory Center for Micro and Nanoscale Research and Fabrication Institute of Advanced Technology University of Science and Technology of China Hefei 230026 P. R. China

F

Fangzhou Jiang

Hefei National Laboratory for Physical Sciences at Microscale and Department of Physics

Z

Zhiqiang Zhu

State Key Laboratory of Chemo and Biosensing, College of Chemistry and Chemical Engineering

F

Fangsheng Huang

Key Laboratory of Precision and Intelligent Chemistry CAS Key Laboratory of Mechanical Behavior and Design of Materials Department of Precision Machinery and Precision Instrumentation National Synchrotron Radiation Laboratory Center for Micro and Nanoscale Research and Fabrication Institute of Advanced Technology University of Science and Technology of China Hefei 230026 P. R. China

C

Chen Li

Sibley School of Mechanical and Aerospace Engineering, Cornell University, Ithaca, NY, USA.

Y

Yaping Li

State Key Laboratory of Chemical Resource Engineering, College of Chemistry

J

Junfa Zhu

National Synchrotron Radiation Laboratory

W

Wangsheng Chu

National Synchrotron Radiation Laboratory

Y

Yue Lin

Y

Yong Ni

CAS Key Laboratory of Mechanical Behavior and Design of Materials, Department of Modern Mechanics, CAS Center for Excellence in Complex System Mechanics

Y

Yi Xie

C

Changzheng Wu

State Key Laboratory of Precision and Intelligent Chemistry, School of Chemistry and Materials Science