Strong, ductile, and hierarchical hetero-lamellar-structured alloys through microstructural inheritance and refinement

P Peijian Shi (State Key Laboratory of Advanced Special Steel, Shanghai Key Laboratory of Advanced Ferromletallurgy, School of Materials Science and Engineering, Shanghai University) Y Yi Li Z Zhi Li X Xin Jiang J Jie Yan R Rui Zhou Y Yi Qin (State Key Laboratory of Advanced Special Steel, Shanghai Key Laboratory of Advanced Ferromletallurgy, School of Materials Science and Engineering, Shanghai University) Y Yifan Lin (State Key Laboratory of Elemento-Organic Chemistry and Frontiers Science Center for New Organic Matter, College of Chemistry) J Jingran Huang (State Key Laboratory of Advanced Special Steel, Shanghai Key Laboratory of Advanced Ferromletallurgy, School of Materials Science and Engineering, Shanghai University) B Bodong Tan (State Key Laboratory of Advanced Special Steel, Shanghai Key Laboratory of Advanced Ferromletallurgy, School of Materials Science and Engineering, Shanghai University) Y Yinan Wang (Department of Information and Computing Sciences, School of Mathematical Science, Peking University) T Tongqi Wen (Department of Mechanical Engineering, The University of Hong Kong) B Beilin Ye (Department of Mechanical Engineering, The University of Hong Kong) C Chunyan Ling (Department of Advanced Design and Systems Engineering, City University of Hong Kong) J Junhua Luan (Department of Materials Science and Engineering, Hong Kong Institute for Advanced Study, City University of Hong Kong) Z Zhe Shen (Department of Neurobiology, School of Biological Sciences, University of California) B Biao Ding (State Key Laboratory of Advanced Special Steel, Shanghai Key Laboratory of Advanced Ferromletallurgy, School of Materials Science and Engineering, Shanghai University) Q Qiang Li T Tianxiang Zheng (College of Science) W Weili Ren (State Key Laboratory of Advanced Special Steel, Shanghai Key Laboratory of Advanced Ferromletallurgy, School of Materials Science and Engineering, Shanghai University) T Tianlong Zhang (Department of Mechanical and Aerospace Engineering) Y Yang Ren Y Yunbo Zhong (State Key Laboratory of Advanced Special Steel, Shanghai Key Laboratory of Advanced Ferromletallurgy, School of Materials Science and Engineering, Shanghai University) C C. T. Liu (Department of Materials Science and Engineering, Hong Kong Institute for Advanced Study, City University of Hong Kong) H Huajian Gao Y Yuntian Zhu (Department of Materials Science and Engineering, Hong Kong Institute for Advanced Study, City University of Hong Kong)

Abstract

The strength−ductility trade-off exists ubiquitously, especially in brittle intermetallic-containing multiple principal element alloys (MPEAs), where the intermetallic phases often induce premature failure leading to severe ductility reduction. Hierarchical heterogeneities represent a promising microstructural solution to achieve simultaneous strength−ductility enhancement. However, it remains fundamentally challenging to tailor hierarchical heterostructures using conventional methods, which often rely on costly and time-consuming processing. Here, we report a multiscale microstructural inheritance and refinement strategy to process “structural hierarchy precursors” in as-cast heterogeneous Al 0.7 CoCrFeNi MPEAs, which lead directly to a hierarchical hetero-lamellar structure (HLS) after simple rolling and annealing. Interestingly, it takes only 10 min of annealing time, two orders of magnitude less than that required to render the state-of-the-art properties during conventional processing of Al 0.7 CoCrFeNi, for us to achieve record-high strength−ductility combinations via the hierarchical HLS design that sequentially stimulates multiple unusual deformation and reinforcement mechanisms. In particular, the HLS-enabled high hetero-deformation-induced (HDI) internal stress triggers profuse <111>-type dislocations on over five independent slip systems in the supposedly brittle intermetallic phase and activates extensive stacking faults (SFs) and nanotwinning in the adjoining soft phase with a rather high SF energy. These unexpected, dynamically reinforcing hetero-deformation mechanisms across multiple length scales facilitate high sustained HDI strain hardening, along with a salient microcrack-mediated extrinsic ductilization effect, suggesting that the proposed microstructural inheritance and refinement strategy provides an efficient, fast, and low-cost approach to overcome the strength−ductility trade-off in a broad range of structural materials.

Article Details

Volume / Issue Vol. 122, Issue 2
Published January 14, 2025
ISSN 0027-8424
Publisher National Academy of Sciences

Authors (26)

P

Peijian Shi

State Key Laboratory of Advanced Special Steel, Shanghai Key Laboratory of Advanced Ferromletallurgy, School of Materials Science and Engineering, Shanghai University

Y

Yi Li

Z

Zhi Li

X

Xin Jiang

J

Jie Yan

R

Rui Zhou

Y

Yi Qin

State Key Laboratory of Advanced Special Steel, Shanghai Key Laboratory of Advanced Ferromletallurgy, School of Materials Science and Engineering, Shanghai University

Y

Yifan Lin

State Key Laboratory of Elemento-Organic Chemistry and Frontiers Science Center for New Organic Matter, College of Chemistry

J

Jingran Huang

State Key Laboratory of Advanced Special Steel, Shanghai Key Laboratory of Advanced Ferromletallurgy, School of Materials Science and Engineering, Shanghai University

B

Bodong Tan

State Key Laboratory of Advanced Special Steel, Shanghai Key Laboratory of Advanced Ferromletallurgy, School of Materials Science and Engineering, Shanghai University

Y

Yinan Wang

Department of Information and Computing Sciences, School of Mathematical Science, Peking University

T

Tongqi Wen

Department of Mechanical Engineering, The University of Hong Kong

B

Beilin Ye

Department of Mechanical Engineering, The University of Hong Kong

C

Chunyan Ling

Department of Advanced Design and Systems Engineering, City University of Hong Kong

J

Junhua Luan

Department of Materials Science and Engineering, Hong Kong Institute for Advanced Study, City University of Hong Kong

Z

Zhe Shen

Department of Neurobiology, School of Biological Sciences, University of California

B

Biao Ding

State Key Laboratory of Advanced Special Steel, Shanghai Key Laboratory of Advanced Ferromletallurgy, School of Materials Science and Engineering, Shanghai University

Q

Qiang Li

T

Tianxiang Zheng

College of Science

W

Weili Ren

State Key Laboratory of Advanced Special Steel, Shanghai Key Laboratory of Advanced Ferromletallurgy, School of Materials Science and Engineering, Shanghai University

T

Tianlong Zhang

Department of Mechanical and Aerospace Engineering

Y

Yang Ren

Y

Yunbo Zhong

State Key Laboratory of Advanced Special Steel, Shanghai Key Laboratory of Advanced Ferromletallurgy, School of Materials Science and Engineering, Shanghai University

C

C. T. Liu

Department of Materials Science and Engineering, Hong Kong Institute for Advanced Study, City University of Hong Kong

H

Huajian Gao

Y

Yuntian Zhu

Department of Materials Science and Engineering, Hong Kong Institute for Advanced Study, City University of Hong Kong