Single‐Molecule Additive Integrating Na‐Ion Reservoir, Cosolvent, and Diluent Functions for Low‐Temperature Na‐Ion Batteries

S Shengfei Wang (State Key Laboratory of Molecular Engineering of Polymers, Department of Macromolecular Science, Institute of Fiber Materials and Devices, Research Center of AI for Polymer Science, Collaborative Innovation Center of Chemistry for Energy Materials) G Guanbin Wu C Chihao Zhao (State Key Laboratory of Molecular Engineering of Polymers Department of Macromolecular Science Institute of Fiber Materials and Devices Research Center of AI For Polymer Science Collaborative Innovation Center of Chemistry for Energy Materials Fudan University Shanghai China) Y Yanlong Zhao (Beijing Key Laboratory of Green Chemical Reaction Engineering and Technology, Department of Chemical Engineering) H Huajing Li (State Key Laboratory of Molecular Engineering of Polymers, Department of Macromolecular Science, Institute of Fiber Materials and Devices, Research Center of AI for Polymer Science, Collaborative Innovation Center of Chemistry for Energy Materials) Z Ziyang Kang (State Key Laboratory of Molecular Engineering of Polymers, Department of Macromolecular Science, Institute of Fiber Materials and Devices, Research Center of AI for Polymer Science, Collaborative Innovation Center of Chemistry for Energy Materials) J Jiayong Du (State Key Laboratory of Molecular Engineering of Polymers Department of Macromolecular Science Institute of Fiber Materials and Devices Research Center of AI For Polymer Science Collaborative Innovation Center of Chemistry for Energy Materials Fudan University Shanghai China) Z Zhengyuan Tang (State Key Laboratory of Molecular Engineering of Polymers Department of Macromolecular Science Institute of Fiber Materials and Devices Research Center of AI For Polymer Science Collaborative Innovation Center of Chemistry for Energy Materials Fudan University Shanghai China) Z Zilong Zheng X Xinwei Du (State Key Laboratory of Molecular Engineering of Polymers, Department of Macromolecular Science, Institute of Fiber Materials and Devices, Research Center of AI for Polymer Science, Collaborative Innovation Center of Chemistry for Energy Materials) W Wenwen Wang X Xiaotian Guo Y Yue Gao

Abstract

ABSTRACT Na‐ion batteries hold great promise for low‐temperature energy storage, but their performance is severely constrained by Na‐ion loss, electrolyte freezing, and elevated viscosity. While each issue demands carefully tailored additive molecules, their combined use often leads to performance interference and complicates the manufacturing process. To overcome these concurrent challenges, we report an organic molecule, NaB(C 2 H 5 ) 4 , designed via machine learning, which incorporates three functional components in a single entity: Na + to replenish sodium inventory, B(C 2 H 5 ) 3 as a low‐freezing‐point cosolvent, and C 4 H 10 as a viscosity‐reducing diluent. NaB(C 2 H 5 ) 4 undergoes complete decomposition below 4.0 V via a free‐radical cleavage pathway, as confirmed by NMR and mass spectrometry. The incorporation of this molecule reduces the freezing point of the ether electrolyte to −85.0°C, and when formulated in an ether‐based electrolyte at −60°C, it achieves an ionic conductivity of 0.61 mS cm −1 and a viscosity of 49.7 mPa s. As a result, the hard carbon||P2‐Na 2/3 Ni 1/3 Fe 1/3 Mn 1/3 O 2 pouch cell exhibits an improved initial Coulombic efficiency from 64.8% to 83.7%, along with 90.2% capacity retention over 200 cycles at −60°C.

Article Details

Volume / Issue Vol. 65, Issue 31
Published July 27, 2026
ISSN 1433-7851
Publisher Wiley

Journal Info

Angewandte Chemie International Edition

Wiley

ISSN: 1433-7851 Physical Sciences

Authors (13)

S

Shengfei Wang

State Key Laboratory of Molecular Engineering of Polymers, Department of Macromolecular Science, Institute of Fiber Materials and Devices, Research Center of AI for Polymer Science, Collaborative Innovation Center of Chemistry for Energy Materials

G

Guanbin Wu

C

Chihao Zhao

State Key Laboratory of Molecular Engineering of Polymers Department of Macromolecular Science Institute of Fiber Materials and Devices Research Center of AI For Polymer Science Collaborative Innovation Center of Chemistry for Energy Materials Fudan University Shanghai China

Y

Yanlong Zhao

Beijing Key Laboratory of Green Chemical Reaction Engineering and Technology, Department of Chemical Engineering

H

Huajing Li

State Key Laboratory of Molecular Engineering of Polymers, Department of Macromolecular Science, Institute of Fiber Materials and Devices, Research Center of AI for Polymer Science, Collaborative Innovation Center of Chemistry for Energy Materials

Z

Ziyang Kang

State Key Laboratory of Molecular Engineering of Polymers, Department of Macromolecular Science, Institute of Fiber Materials and Devices, Research Center of AI for Polymer Science, Collaborative Innovation Center of Chemistry for Energy Materials

J

Jiayong Du

State Key Laboratory of Molecular Engineering of Polymers Department of Macromolecular Science Institute of Fiber Materials and Devices Research Center of AI For Polymer Science Collaborative Innovation Center of Chemistry for Energy Materials Fudan University Shanghai China

Z

Zhengyuan Tang

State Key Laboratory of Molecular Engineering of Polymers Department of Macromolecular Science Institute of Fiber Materials and Devices Research Center of AI For Polymer Science Collaborative Innovation Center of Chemistry for Energy Materials Fudan University Shanghai China

Z

Zilong Zheng

X

Xinwei Du

State Key Laboratory of Molecular Engineering of Polymers, Department of Macromolecular Science, Institute of Fiber Materials and Devices, Research Center of AI for Polymer Science, Collaborative Innovation Center of Chemistry for Energy Materials

W

Wenwen Wang

X

Xiaotian Guo

Y

Yue Gao