Recyclable Quasi‐Homogeneous Carbon Nitride Colloidal Catalyst for Sustainable Photocatalytic H <sub>2</sub> O <sub>2</sub> Generation

L Lian‐Lian Liu (Department of Environmental Science and Engineering University of Science and Technology of China Hefei 230026 P.R. China) C Chao Cui F Fei Chen J Jie‐Jie Chen (State Key Laboratory of Advanced Environmental Technology Department of Environmental Science and Engineering University of Science and Technology of China Hefei Anhui 230026 P.R. China) H Han‐Qing Yu (State Key Laboratory of Advanced Environmental Technology Department of Environmental Science and Engineering University of Science and Technology of China Hefei Anhui 230026 P.R. China) Y Yujie Xiong (State Key Laboratory of Advanced Glass Materials, Anhui Engineering Research Center of Carbon Neutrality, The Key Laboratory of Functional Molecular Solids, Ministry of Education, Anhui Laboratory of Molecular-Based Materials, College of Chemistry and Materials Science)

Abstract

Abstract Graphitic carbon nitride (g‐C 3 N 4 ) photocatalysts have attracted growing interest for the eco‐friendly, solar‐driven synthesis of hydrogen peroxide (H 2 O 2 ). However, the catalytic efficiency remains limited by poor accessibility of reactive sites due to the hydrophobic nature and aggregation tendency of conventional g‐C 3 N 4 . Here, we report a hydrophilic g‐C 3 N 4 colloidal photocatalyst, synthesized via potassium ion (K⁺) incorporation and surface grafting with sulfonylcyanide groups, which enables quasi‐homogeneous photocatalytic H 2 O 2 production (7,886 µmol g⁻¹ h⁻¹), surpassing most reported g‐C 3 N 4 ‐based heterogeneous systems. The sulfonylcyanide groups facilitate O 2 adsorption and reduction, while synergistically promoting charge separation in conjunction with K⁺ ions. This work demonstrates the potential of hydrophilic g‐C 3 N 4 colloids in quasi‐homogeneous catalysis and presents a versatile strategy for designing advanced g‐C 3 N 4 ‐based photocatalysts for sustainable chemical synthesis.

Article Details

Volume / Issue Vol. 64, Issue 33
Published August 11, 2025
ISSN 1433-7851
Publisher Wiley

Journal Info

Angewandte Chemie International Edition

Wiley

ISSN: 1433-7851 Physical Sciences

Authors (6)

L

Lian‐Lian Liu

Department of Environmental Science and Engineering University of Science and Technology of China Hefei 230026 P.R. China

C

Chao Cui

F

Fei Chen

J

Jie‐Jie Chen

State Key Laboratory of Advanced Environmental Technology Department of Environmental Science and Engineering University of Science and Technology of China Hefei Anhui 230026 P.R. China

H

Han‐Qing Yu

State Key Laboratory of Advanced Environmental Technology Department of Environmental Science and Engineering University of Science and Technology of China Hefei Anhui 230026 P.R. China

Y

Yujie Xiong

State Key Laboratory of Advanced Glass Materials, Anhui Engineering Research Center of Carbon Neutrality, The Key Laboratory of Functional Molecular Solids, Ministry of Education, Anhui Laboratory of Molecular-Based Materials, College of Chemistry and Materials Science