Promoting Electrochemical Reactions with Dual‐Atom Catalysts for High‐Rate Lithium–Sulfur Batteries

J Jing Yu (Institute for Digital Molecular Analytics and Science (IDMxS), Nanyang Technological University, 59 Nanyang Drive, Singapore 636921, Singapore) O Oleg Usoltsev (CELLS‐ALBA Synchrotron Cerdanyola del Vallès Carrer de la Llum, 2, 26 Barcelona Catalonia 08290 Spain) I Irina Martynova (Catalonia Institute for Energy Research (IREC) Sant Adrià de Besòs Barcelona Catalonia 08930 Spain) C Chen Huang (Catalonia Institute for Energy Research-IREC, Sant Adrià de Besòs, Barcelona 08930, Spain) Z Zhifu Liang (College of Ocean Science and Engineering Shanghai Maritime University Shanghai 201306 China) I Ivan Pinto‐Huguet (Catalan Institute of Nanoscience and Nanotechnology – ICN2 (CSIC and BIST) Campus UAB Bellaterra Barcelona 08193 Catalonia Spain) C Canhuang Li (Catalonia Institute for Energy Research-IREC, Sant Adrià de Besòs, Barcelona 08930, Spain) L Liqiang Lu (Helmholtz‐Zentrum Berlin für Materialien und Energie Hahn‐Meitner‐Platz 1 14109 Berlin Germany) C Chaoqi Zhang (Shanghai University , , ,) X Xuan Lu K Kapil Gupta M Marc Botifoll L Laura Simonelli (CELLS─ALBA Synchrotron Radiation Facility, Carrer de la Llum 2-26, Cerdanyola del Vallès 08290, Spain) F Francois Fauth (CELLS-ALBA Synchrotron, Cerdanyola del Vallès, E-08290 Barcelona, Spain) J Jin Yuan Zhou (School of Physical Science & Technology) J Jordi Llorca (Department of Chemical Engineering and Center for Research in Multiscale Science and Engineering, Universitat Politècnica de Catalunya, UPC-EEBE, Eduard Maristany 10-14, 08019 Barcelona, Spain) Y Yan Lu C Chao Yue Zhang (Department of Chemistry and Biochemistry) J Jordi Arbiol (Catalan Institute of Nanoscience and Nanotechnology − ICN2 (CSIC and BIST), Campus UAB, Bellaterra, Barcelona, Catalonia 08193, Spain) A Andreu Cabot (Catalonia Institute for Energy Research-IREC, Sant Adrià de Besòs, Barcelona 08930, Spain)

Abstract

Abstract Sulfur cathodes offer a promising solution for high‐energy‐density, cost‐effective, and sustainable energy storage. However, their practical application is limited by sluggish and complex multistep sulfur redox reactions (SRRs), involving both electrochemical and chemical processes. Herein, it is demonstrated that accelerating electrochemical processes, particularly Li 2 S nucleation, over competing chemical pathways is fundamental to minimizing sulfur loss and achieving high‐rate performance. To this end, a scalable and cost‐effective strategy is presented for synthesizing a series of 3d transition metal–bismuth (TM–Bi) atomic pairs anchored on carbon nitride (CN) and investigate their potential to activate SRRs in lithium‐sulfur batteries (LSBs). An initial screening identifies Ni–Bi/CN and Co–Bi/CN as highly effective in improving rate performance. Detailed analysis shows these catalysts promote direct electrochemical transitions and rapid Li 2 S nucleation over competing chemical reactions, enabling high charge–discharge rates while preventing active material loss and enhancing stability. Electrochemical analysis, density functional theory, and operando spectroscopy reveal that TM‐Bi pairing shifts d‐band states closer to the Fermi level and modulates HOMO–LUMO levels, promoting lithium polysulfide (LiPS) interaction and facilitating efficient charge transfer. These findings offer valuable insights for designing advanced catalysts for LSBs and broader electrocatalytic applications.

Article Details

Volume / Issue Vol. 38, Issue 2
Published January 01, 2026
ISSN 0935-9648
Publisher Unknown Publisher

Journal Info

Advanced Materials

Unknown Publisher

ISSN: 0935-9648 Physical Sciences

Authors (20)

J

Jing Yu

Institute for Digital Molecular Analytics and Science (IDMxS), Nanyang Technological University, 59 Nanyang Drive, Singapore 636921, Singapore

O

Oleg Usoltsev

CELLS‐ALBA Synchrotron Cerdanyola del Vallès Carrer de la Llum, 2, 26 Barcelona Catalonia 08290 Spain

I

Irina Martynova

Catalonia Institute for Energy Research (IREC) Sant Adrià de Besòs Barcelona Catalonia 08930 Spain

C

Chen Huang

Catalonia Institute for Energy Research-IREC, Sant Adrià de Besòs, Barcelona 08930, Spain

Z

Zhifu Liang

College of Ocean Science and Engineering Shanghai Maritime University Shanghai 201306 China

I

Ivan Pinto‐Huguet

Catalan Institute of Nanoscience and Nanotechnology – ICN2 (CSIC and BIST) Campus UAB Bellaterra Barcelona 08193 Catalonia Spain

C

Canhuang Li

Catalonia Institute for Energy Research-IREC, Sant Adrià de Besòs, Barcelona 08930, Spain

L

Liqiang Lu

Helmholtz‐Zentrum Berlin für Materialien und Energie Hahn‐Meitner‐Platz 1 14109 Berlin Germany

C

Chaoqi Zhang

Shanghai University , , ,

X

Xuan Lu

K

Kapil Gupta

M

Marc Botifoll

L

Laura Simonelli

CELLS─ALBA Synchrotron Radiation Facility, Carrer de la Llum 2-26, Cerdanyola del Vallès 08290, Spain

F

Francois Fauth

CELLS-ALBA Synchrotron, Cerdanyola del Vallès, E-08290 Barcelona, Spain

J

Jin Yuan Zhou

School of Physical Science & Technology

J

Jordi Llorca

Department of Chemical Engineering and Center for Research in Multiscale Science and Engineering, Universitat Politècnica de Catalunya, UPC-EEBE, Eduard Maristany 10-14, 08019 Barcelona, Spain

Y

Yan Lu

C

Chao Yue Zhang

Department of Chemistry and Biochemistry

J

Jordi Arbiol

Catalan Institute of Nanoscience and Nanotechnology − ICN2 (CSIC and BIST), Campus UAB, Bellaterra, Barcelona, Catalonia 08193, Spain

A

Andreu Cabot

Catalonia Institute for Energy Research-IREC, Sant Adrià de Besòs, Barcelona 08930, Spain