Programmable Diacetylene‐Bridged Cyclotetrathiophenes With Nonplanar π‐Expanded Skeleton for Electrochemical Sodium Storage

H Honghui Hu (National Base for International Science & Technology Cooperation Key Laboratory of Environmentally Friendly Chemistry and Application of Ministry of Education, School of Chemistry Xiangtan University Xiangtan P. R. China) Y Yu Mei (College of Chemistry and Chemical Engineering) M Mingjun Jing (National Base for International Science & Technology Cooperation Key Laboratory of Environmentally Friendly Chemistry and Application of Ministry of Education, School of Chemistry Xiangtan University Xiangtan P. R. China) J Jinyang Wu (National Base for International Science & Technology Cooperation Key Laboratory of Environmentally Friendly Chemistry and Application of Ministry of Education, School of Chemistry Xiangtan University Xiangtan P. R. China) T Tianjing Wu (National Base for International Science & Technology Cooperation Key Laboratory of Environmentally Friendly Chemistry and Application of Ministry of Education, School of Chemistry Xiangtan University Xiangtan P. R. China) J Jinzhi Yuan (National Base for International Science & Technology Cooperation Key Laboratory of Environmentally Friendly Chemistry and Application of Ministry of Education, School of Chemistry Xiangtan University Xiangtan P. R. China) Z Zichun Zhang (Institute of Chemical Biology) Y Yong Pei (Department of Chemistry, Key Laboratory of Environmentally Friendly Chemistry and Applications of MOE, Xiangtan University, Xiangtan 411105, China) C Cheng Cheng Y Yujie Huang (State Key Laboratory for Chemistry and Molecular Engineering of Medicinal Resources/Key Laboratory for Chemistry and Molecular Engineering of Medicinal Resources (Ministry of Education of China), Collaborative Innovation Center for Guangxi Ethnic Medicine, School of Chemistry and Pharmaceutical Sciences) H Hongshuai Hou (College of Chemistry and Chemical Engineering) X Xianyou Wang (National Base for International Science & Technology Cooperation Key Laboratory of Environmentally Friendly Chemistry and Application of Ministry of Education, School of Chemistry Xiangtan University Xiangtan P. R. China) X Xiaobo Ji (College of Chemistry and Chemical Engineering)

Abstract

ABSTRACT Fused aromatic ring systems offer flexibility in molecular‐level design, facilitating programmable redox activity and exhibiting remarkable energy‐storage performance. Nevertheless, the planar backbone structure and strong π–π stacking significantly impede their practical capacity and cycle stability. Herein, we present a novel three‐dimensional (3D) polymer, diacetylene‐linked cyclic tetrathiophene ( 3D‐PTE‐COTh ) with a partial crystalline structure, which is based on the thiophene‐fused [8]cycloene framework and intramolecular acetylene connecting wires. This construction exploits the electrochemically induced micro‐telescopic behavior regulated by Hückel's rule, allowing for dynamic conformational alterations that alleviate π–π stacking effects. Simultaneously, the combination of fused thiophene and graphdiyne‐like linkages improves electronic conductivity and introduces a plethora of electron‐deficient redox‐active sites. As a cathode material, the synergistic sodium storage of the cyclooctatetraene (C 8 ring), ─C≡C─C≡C─ bonds, and fused‐thiophene enables 3D‐PTE‐COTh to achieve a high specific capacity of 347.9 mAh g −1 at 0.5 A g −1 , thereby presenting new prospects for the design of advanced organic electrode materials.

Article Details

Volume / Issue Vol. 65, Issue 21
Published May 18, 2026
ISSN 1433-7851
Publisher Wiley

Journal Info

Angewandte Chemie International Edition

Wiley

ISSN: 1433-7851 Physical Sciences

Authors (13)

H

Honghui Hu

National Base for International Science & Technology Cooperation Key Laboratory of Environmentally Friendly Chemistry and Application of Ministry of Education, School of Chemistry Xiangtan University Xiangtan P. R. China

Y

Yu Mei

College of Chemistry and Chemical Engineering

M

Mingjun Jing

National Base for International Science & Technology Cooperation Key Laboratory of Environmentally Friendly Chemistry and Application of Ministry of Education, School of Chemistry Xiangtan University Xiangtan P. R. China

J

Jinyang Wu

National Base for International Science & Technology Cooperation Key Laboratory of Environmentally Friendly Chemistry and Application of Ministry of Education, School of Chemistry Xiangtan University Xiangtan P. R. China

T

Tianjing Wu

National Base for International Science & Technology Cooperation Key Laboratory of Environmentally Friendly Chemistry and Application of Ministry of Education, School of Chemistry Xiangtan University Xiangtan P. R. China

J

Jinzhi Yuan

National Base for International Science & Technology Cooperation Key Laboratory of Environmentally Friendly Chemistry and Application of Ministry of Education, School of Chemistry Xiangtan University Xiangtan P. R. China

Z

Zichun Zhang

Institute of Chemical Biology

Y

Yong Pei

Department of Chemistry, Key Laboratory of Environmentally Friendly Chemistry and Applications of MOE, Xiangtan University, Xiangtan 411105, China

C

Cheng Cheng

Y

Yujie Huang

State Key Laboratory for Chemistry and Molecular Engineering of Medicinal Resources/Key Laboratory for Chemistry and Molecular Engineering of Medicinal Resources (Ministry of Education of China), Collaborative Innovation Center for Guangxi Ethnic Medicine, School of Chemistry and Pharmaceutical Sciences

H

Hongshuai Hou

College of Chemistry and Chemical Engineering

X

Xianyou Wang

National Base for International Science & Technology Cooperation Key Laboratory of Environmentally Friendly Chemistry and Application of Ministry of Education, School of Chemistry Xiangtan University Xiangtan P. R. China

X

Xiaobo Ji

College of Chemistry and Chemical Engineering