Polymer Ligands with Quaternary Ammonium Binding Motifs on Metal Nanoparticles Enable Selective Ion Transport for CO <sub>2</sub> Electroreduction

D Debasmita Muhuri (Department of Chemistry, University of Connecticut Department of Chemistry University of Connecticut Storrs Connecticut 06269 USA) M Manthan Sarkar (Department of Chemistry, University of Connecticut Department of Chemistry University of Connecticut Storrs Connecticut 06269 USA) H Hanyi Duan (Department of Chemistry) L Lindsey A. Hanson (Department of Chemistry Trinity College Hartford Connecticut 06106 USA) J Jie He (Department of Chemistry)

Abstract

Abstract We report a new class of hydrophobic polymer ligands with quaternary ammonium head groups for surface modification of noble metal nanoparticles (NPs). Quaternary ammonium ligands bind NPs through non‐covalent electrostatic interactions, producing polymer‐grafted NPs with high colloidal and chemical stability. These polymers having charged head groups offer powerful strategies to tailor the structure and function of metal‐electrolyte interfaces in electrocatalytic systems. The ammonium head groups serve as ionic reservoirs that preconcentrate bicarbonate counterions at the surface of nanocatalysts, while the hydrophobic polymer backbones restructure local hydrogen‐bonding networks, modulating water and ion transport dynamics. These interfacial effects promote CO 2 electroreduction, particularly under diffusion‐limited conditions, resulting in a CO Faradaic efficiency (FE) exceeding 90%.

Article Details

Volume / Issue Vol. 64, Issue 45
Published November 03, 2025
ISSN 1433-7851
Publisher Wiley

Journal Info

Angewandte Chemie International Edition

Wiley

ISSN: 1433-7851 Physical Sciences

Authors (5)

D

Debasmita Muhuri

Department of Chemistry, University of Connecticut Department of Chemistry University of Connecticut Storrs Connecticut 06269 USA

M

Manthan Sarkar

Department of Chemistry, University of Connecticut Department of Chemistry University of Connecticut Storrs Connecticut 06269 USA

H

Hanyi Duan

Department of Chemistry

L

Lindsey A. Hanson

Department of Chemistry Trinity College Hartford Connecticut 06106 USA

J

Jie He

Department of Chemistry