Native metabolomics identifies pteridines as CutA ligands and modulators of copper binding

B Berenike C. Wagner (Department of Organismic Interactions, Interfaculty Institute of Microbiology and Infection Medicine, University of Tübingen) K Karoline Steuer-Lodd (Department of Biochemistry, University of California) C Christian Geibel (Cluster of Excellence “Controlling Microbes to Fight Infections” (Excellence Cluster 2124), Interfaculty Institute of Microbiology and Infection Medicine, University of Tübingen) A Amelie Stadelmann (Cluster of Excellence “Controlling Microbes to Fight Infections” (Excellence Cluster 2124), Interfaculty Institute of Microbiology and Infection Medicine, University of Tübingen) J Johanna Rapp (Cluster of Excellence “Controlling Microbes to Fight Infections” (Excellence Cluster 2124), Interfaculty Institute of Microbiology and Infection Medicine, University of Tübingen) H Hannes Link (Cluster of Excellence “Controlling Microbes to Fight Infections” (Excellence Cluster 2124), Interfaculty Institute of Microbiology and Infection Medicine, University of Tübingen) T Tilman Schramm (Department of Biochemistry, University of California) N Nouneh Boodaghian (Department of Microbiology and Plant Pathology, University of California) A Ansel Hsiao (Department of Microbiology and Plant Pathology, University of California) E Eva Nussbaum (Department of Organismic Interactions, Interfaculty Institute of Microbiology and Infection Medicine, University of Tübingen) H Heinz-Paul Grenzendorfer (Department of Organismic Interactions, Interfaculty Institute of Microbiology and Infection Medicine, University of Tübingen) R Reinhard Albrecht (Department of Protein Evolution, Max Planck Institute for Developmental Biology) M Marcus D. Hartmann (Department of Protein Evolution, Max Planck Institute for Developmental Biology) K Karl Forchhammer (Department of Organismic Interactions, Interfaculty Institute of Microbiology and Infection Medicine, University of Tübingen) K Khaled A. Selim (Microbial Biochemistry Group, Institute of Phototrophic Microbiology, Faculty of Mathematics and Natural Sciences, Heinrich-Heine University Düsseldorf) C Chambers C. Hughes (Cluster of Excellence “Controlling Microbes to Fight Infections” (Excellence Cluster 2124), Interfaculty Institute of Microbiology and Infection Medicine, University of Tübingen) D Daniel Petras (Cluster of Excellence “Controlling Microbes to Fight Infections” (Excellence Cluster 2124), Interfaculty Institute of Microbiology and Infection Medicine, University of Tübingen)

Abstract

CutA, a conserved protein across all domains of life, has been suggested to be involved in copper tolerance in bacteria, though recent studies have questioned this association, leaving its biological role unknown. To clarify its function, we studied cutA knockout mutants from two phylogenetically distant species, Synechococcus elongatus PCC 7942 and Escherichia coli , using phenotyping combined with metabolomics. To investigate the interaction of CutA with potential substrates and cofactors, we performed a series of native metabolomics experiments with CutA and cell extracts from which we identified the lumazine 2’-deoxyxanthopterin B2, a previously uncharacterized pteridine, to bind CutA in both species. Based on these results, we identified a set of other pteridines, including the essential cofactor tetrahydrobiopterin, as ligands of CutA. In the presence of pterins, we observed an increased affinity of CutA for copper ions. In addition, E. coli CutA mutants exhibited decreased copper resistance. These findings, alongside the known role of pteridines as redox shuttles, suggest a previously unrecognized role for CutA in coordinating cellular copper homeostasis and redox balance via pteridine metabolism.

Article Details

Volume / Issue Vol. 122, Issue 48
Published December 02, 2025
ISSN 0027-8424
Publisher National Academy of Sciences

Authors (17)

B

Berenike C. Wagner

Department of Organismic Interactions, Interfaculty Institute of Microbiology and Infection Medicine, University of Tübingen

K

Karoline Steuer-Lodd

Department of Biochemistry, University of California

C

Christian Geibel

Cluster of Excellence “Controlling Microbes to Fight Infections” (Excellence Cluster 2124), Interfaculty Institute of Microbiology and Infection Medicine, University of Tübingen

A

Amelie Stadelmann

Cluster of Excellence “Controlling Microbes to Fight Infections” (Excellence Cluster 2124), Interfaculty Institute of Microbiology and Infection Medicine, University of Tübingen

J

Johanna Rapp

Cluster of Excellence “Controlling Microbes to Fight Infections” (Excellence Cluster 2124), Interfaculty Institute of Microbiology and Infection Medicine, University of Tübingen

H

Hannes Link

Cluster of Excellence “Controlling Microbes to Fight Infections” (Excellence Cluster 2124), Interfaculty Institute of Microbiology and Infection Medicine, University of Tübingen

T

Tilman Schramm

Department of Biochemistry, University of California

N

Nouneh Boodaghian

Department of Microbiology and Plant Pathology, University of California

A

Ansel Hsiao

Department of Microbiology and Plant Pathology, University of California

E

Eva Nussbaum

Department of Organismic Interactions, Interfaculty Institute of Microbiology and Infection Medicine, University of Tübingen

H

Heinz-Paul Grenzendorfer

Department of Organismic Interactions, Interfaculty Institute of Microbiology and Infection Medicine, University of Tübingen

R

Reinhard Albrecht

Department of Protein Evolution, Max Planck Institute for Developmental Biology

M

Marcus D. Hartmann

Department of Protein Evolution, Max Planck Institute for Developmental Biology

K

Karl Forchhammer

Department of Organismic Interactions, Interfaculty Institute of Microbiology and Infection Medicine, University of Tübingen

K

Khaled A. Selim

Microbial Biochemistry Group, Institute of Phototrophic Microbiology, Faculty of Mathematics and Natural Sciences, Heinrich-Heine University Düsseldorf

C

Chambers C. Hughes

Cluster of Excellence “Controlling Microbes to Fight Infections” (Excellence Cluster 2124), Interfaculty Institute of Microbiology and Infection Medicine, University of Tübingen

D

Daniel Petras

Cluster of Excellence “Controlling Microbes to Fight Infections” (Excellence Cluster 2124), Interfaculty Institute of Microbiology and Infection Medicine, University of Tübingen