Ligand Engineering for Precise Control of Ultrathin CsPbI <sub>3</sub> Nanoplatelet Superlattices for Efficient Light‐Emitting Diodes

J Jongbeom Kim (Department of Materials Science and Engineering Ulsan National Institute of Science and Technology (UNIST) Ulsan Republic of Korea) W Woo Hyeon Jeong J Junzhi Ye A Allison Nicole Arber (Department of Materials University of Oxford Oxford UK) V Vikram (Department of Materials University of Oxford Oxford UK) D Donghan Kim (School of Electronic and Electrical Engineering, Kyungpook National University 1 , Daegu 41566,) Y Yi‐Teng Huang (Inorganic Chemistry Laboratory University of Oxford Oxford UK) Y Yixin Wang (State Key Laboratory of Molecular Engineering of Polymers) D Dongeun Kim (Department of Materials Science and Engineering Ulsan National Institute of Science and Technology (UNIST) Ulsan Republic of Korea) D Dongryeol Lee (Department of Materials Science and Engineering Ulsan National Institute of Science and Technology (UNIST) Ulsan Republic of Korea) C Chia‐Yu Chang (Sustainable Electrochemical Energy Development Center (SEED Center) National Taiwan University of Science and Technology Taipei Taiwan) X Xinyu Shen S Sung Yong Bae (Inorganic Chemistry Laboratory University of Oxford Oxford UK) A Ashish Gaurav (Inorganic Chemistry Laboratory University of Oxford Oxford UK) Y Ye In Kim (Department of Materials Science and Engineering Ulsan National Institute of Science and Technology (UNIST) Ulsan Republic of Korea) J Jinkyu Yang (Department of Materials Science and Engineering Ulsan National Institute of Science and Technology (UNIST) Ulsan Republic of Korea) B Boseung Je (Department of Materials Science and Engineering Pohang University of Science and Technology (POSTECH) Pohang Republic of Korea) C Changsoon Cho (Department of Materials Science and Engineering Pohang University of Science and Technology (POSTECH) Pohang Republic of Korea) A Akshay Rao H Henry J. Snaith M M. Saiful Islam B Bo Ram Lee (School of Advanced Materials Science and Engineering) M Myoung Hoon Song (Department of Materials Science and Engineering Ulsan National Institute of Science and Technology (UNIST) Ulsan Republic of Korea) R Robert L. Z. Hoye

Abstract

ABSTRACT Strongly‐confined perovskite nanoplatelets (PeNPLs) offer opportunities not found in conventional isotropic nanocubes, especially in producing linearly polarized light, as well as enhancing outcoupling through control over the transition dipole moment. But this requires ultrathin nanoplatelets with three or fewer monolayers of PbI 6 octahedra across the thickness, which are challenging to synthesise uniformly, and their luminescence is strongly affected by surface defects. Together, these limit the performance of ultrathin PeNPLs in light‐emitting diodes (LEDs). Here, we address these challenges with an ancillary ligand engineering strategy. We demonstrate that ligands with phosphoryl functional groups strongly bind to the perovskite surface, while having an organic backbone that is not sterically bulky ensures high ligand density. By modulating nucleation and growth, these ancillary ligands lead to monodisperse PeNPLs that stack more uniformly when self‐assembled into superlattices, with suppressed agglomeration. As a result, from edge‐up PeNPL superlattices, we achieve an enhanced degree of polarization, while from face‐down PeNPL superlattices, we achieve enhanced outcoupling that results in LEDs with 13.1% external quantum efficiency, the highest reported for ultrathin PeNPL LEDs. This work establishes ancillary ligand‐induced synthesis as a decisive route to achieve uniform nanoplatelets with robust orientation control, enabling full utilization of the multifunctionality of anisotropic PeNPLs.

Article Details

Volume / Issue Vol. 38, Issue 46
Published August 01, 2026
ISSN 0935-9648
Publisher Unknown Publisher

Journal Info

Advanced Materials

Unknown Publisher

ISSN: 0935-9648 Physical Sciences

Authors (24)

J

Jongbeom Kim

Department of Materials Science and Engineering Ulsan National Institute of Science and Technology (UNIST) Ulsan Republic of Korea

W

Woo Hyeon Jeong

J

Junzhi Ye

A

Allison Nicole Arber

Department of Materials University of Oxford Oxford UK

V

Vikram

Department of Materials University of Oxford Oxford UK

D

Donghan Kim

School of Electronic and Electrical Engineering, Kyungpook National University 1 , Daegu 41566,

Y

Yi‐Teng Huang

Inorganic Chemistry Laboratory University of Oxford Oxford UK

Y

Yixin Wang

State Key Laboratory of Molecular Engineering of Polymers

D

Dongeun Kim

Department of Materials Science and Engineering Ulsan National Institute of Science and Technology (UNIST) Ulsan Republic of Korea

D

Dongryeol Lee

Department of Materials Science and Engineering Ulsan National Institute of Science and Technology (UNIST) Ulsan Republic of Korea

C

Chia‐Yu Chang

Sustainable Electrochemical Energy Development Center (SEED Center) National Taiwan University of Science and Technology Taipei Taiwan

X

Xinyu Shen

S

Sung Yong Bae

Inorganic Chemistry Laboratory University of Oxford Oxford UK

A

Ashish Gaurav

Inorganic Chemistry Laboratory University of Oxford Oxford UK

Y

Ye In Kim

Department of Materials Science and Engineering Ulsan National Institute of Science and Technology (UNIST) Ulsan Republic of Korea

J

Jinkyu Yang

Department of Materials Science and Engineering Ulsan National Institute of Science and Technology (UNIST) Ulsan Republic of Korea

B

Boseung Je

Department of Materials Science and Engineering Pohang University of Science and Technology (POSTECH) Pohang Republic of Korea

C

Changsoon Cho

Department of Materials Science and Engineering Pohang University of Science and Technology (POSTECH) Pohang Republic of Korea

A

Akshay Rao

H

Henry J. Snaith

M

M. Saiful Islam

B

Bo Ram Lee

School of Advanced Materials Science and Engineering

M

Myoung Hoon Song

Department of Materials Science and Engineering Ulsan National Institute of Science and Technology (UNIST) Ulsan Republic of Korea

R

Robert L. Z. Hoye