Internally BN‐Doped Coronene

J Jing‐Cai Zeng (Beijing National Laboratory for Molecular Sciences (BNLMS) Key Laboratory of Bioorganic Chemistry and Molecular Engineering of Ministry of Education Center of Soft Matter Science and Engineering College of Chemistry and Molecular Engineering Peking University Beijing 100871 P.R. China) X Xuan‐Yu Song (Beijing National Laboratory for Molecular Sciences (BNLMS) Key Laboratory of Bioorganic Chemistry and Molecular Engineering of Ministry of Education Center of Soft Matter Science and Engineering College of Chemistry and Molecular Engineering Peking University Beijing 100871 P.R. China) Z Ze‐Fan Yao (Beijing National Laboratory For Molecular Sciences (BNLMS) Key Laboratory of Polymer Chemistry and Physics of Ministry of Education Center For Soft Matter Science and Engineering College of Chemistry and Molecular Engineering Peking University Beijing China) Y Yong‐Shi Chen (Beijing National Laboratory of Molecular Sciences (BNLMS) College of Chemistry and Molecular Engineering Peking University Beijing 100871 China) Y Yu‐Chun Xu (Beijing National Laboratory for Molecular Sciences (BNLMS) Key Laboratory of Bioorganic Chemistry and Molecular Engineering of Ministry of Education Center of Soft Matter Science and Engineering College of Chemistry and Molecular Engineering Peking University Beijing 100871 P.R. China) K Kexiang Zhao (Department of Materials Science and Engineering, Institute of Science Tokyo, 2-12-1 Ookayama, Meguro-ku, Tokyo 152-8552, Japan) Y Yi Liu J Jie‐Yu Wang (Beijing National Laboratory of Molecular Sciences (BNLMS) College of Chemistry and Molecular Engineering Peking University Beijing 100871 China) J Jian Pei

Abstract

Abstract We present the first synthesis of internally BN‐doped coronenes ( B2N2‐C , H‐B2N2‐C , and 2H‐B2N2‐C ) with two covalent B─N units embedded on the central axis of coronene. The B─N doping leads to unique electronic structures with distinct charge distribution, conjugation, aromaticity, and photophysical properties. The structures were successfully identified by the single‐crystal X‐ray scattering. B2N2‐C without sidechains retains the structure of coronene but exhibits stronger π–π stacking, higher electronic coupling, and a narrowed solid‐state bandgap. Driven by the B─N dipole–dipole interaction, all B2N2‐coronene derivatives exhibit more ordered assembly with excimer emission in solution, which is absent in coronene. Notably, two stable polymorphs emerge in single crystals of 2H‐B2N2‐C with two hexyl chains: a kinetically stable rod phase and a thermodynamically stable plate phase, where variations in processing conditions direct the formation of different phases.

Article Details

Volume / Issue Vol. 64, Issue 33
Published August 11, 2025
ISSN 1433-7851
Publisher Wiley

Journal Info

Angewandte Chemie International Edition

Wiley

ISSN: 1433-7851 Physical Sciences

Authors (9)

J

Jing‐Cai Zeng

Beijing National Laboratory for Molecular Sciences (BNLMS) Key Laboratory of Bioorganic Chemistry and Molecular Engineering of Ministry of Education Center of Soft Matter Science and Engineering College of Chemistry and Molecular Engineering Peking University Beijing 100871 P.R. China

X

Xuan‐Yu Song

Beijing National Laboratory for Molecular Sciences (BNLMS) Key Laboratory of Bioorganic Chemistry and Molecular Engineering of Ministry of Education Center of Soft Matter Science and Engineering College of Chemistry and Molecular Engineering Peking University Beijing 100871 P.R. China

Z

Ze‐Fan Yao

Beijing National Laboratory For Molecular Sciences (BNLMS) Key Laboratory of Polymer Chemistry and Physics of Ministry of Education Center For Soft Matter Science and Engineering College of Chemistry and Molecular Engineering Peking University Beijing China

Y

Yong‐Shi Chen

Beijing National Laboratory of Molecular Sciences (BNLMS) College of Chemistry and Molecular Engineering Peking University Beijing 100871 China

Y

Yu‐Chun Xu

Beijing National Laboratory for Molecular Sciences (BNLMS) Key Laboratory of Bioorganic Chemistry and Molecular Engineering of Ministry of Education Center of Soft Matter Science and Engineering College of Chemistry and Molecular Engineering Peking University Beijing 100871 P.R. China

K

Kexiang Zhao

Department of Materials Science and Engineering, Institute of Science Tokyo, 2-12-1 Ookayama, Meguro-ku, Tokyo 152-8552, Japan

Y

Yi Liu

J

Jie‐Yu Wang

Beijing National Laboratory of Molecular Sciences (BNLMS) College of Chemistry and Molecular Engineering Peking University Beijing 100871 China

J

Jian Pei