Interfacial Charge‐Transfer Kinetics Regulate Na <sub>2</sub> S Deposition by Recycled V Single‐Atom Catalysts for Durable Na–S Batteries

G Guangxuan Wu (School of Energy (National Industry‐Education Platform for Energy Storage) School of Materials Science and Engineering and Tianjin Key Laboratory of Composite and Functional Materials Tianjin University Tianjin People's Republic of China) Z Zhihui Zhou (State Key Laboratory of Physical Chemistry of Solid Surfaces, Key Laboratory for Chemical Biology of Fujian Province, The MOE Key Laboratory of Spectrochemical Analysis and Instrumentation, Department of Chemical Biology, College of Chemistry and Chemical Engineering, State Key Laboratory of Vaccines for Infectious Diseases, Fujian Provincial Key Laboratory of Innovative Drug Target Research, School of Pharmaceutical Sciences, School of Life Sciences, Faculty of Medicine and Life Sciences) Y Yeteng Lu (School of Energy (National Industry‐Education Platform for Energy Storage) School of Materials Science and Engineering and Tianjin Key Laboratory of Composite and Functional Materials Tianjin University Tianjin People's Republic of China) Z Zhoujie Lao Y Yuhan Ma N Nan Xiao (School of Energy (National Industry‐Education Platform for Energy Storage) School of Materials Science and Engineering and Tianjin Key Laboratory of Composite and Functional Materials Tianjin University Tianjin People's Republic of China) N Ning Wang C Congqin Zheng (Suzhou Nuclear Power Research Institute Jiangsu People's Republic of China) S Shuiyong Wang (Suzhou Nuclear Power Research Institute Jiangsu People's Republic of China) E Enzuo Liu (School of Materials Science and Engineering and Tianjin Key Laboratory of Composites and Functional Materials) X Xiang Zhang C Chunsheng Shi (School of Energy (National Industry‐Education Platform for Energy Storage) School of Materials Science and Engineering and Tianjin Key Laboratory of Composite and Functional Materials Tianjin University Tianjin People's Republic of China) C Chunnian He W Wenbin Hu N Naiqin Zhao W Wanxiang Zhao (Suzhou Nuclear Power Research Institute Jiangsu People's Republic of China) B Biao Chen (Department of Chemical Physics, School of Chemistry and Materials Science, Hefei National Research Center for Physical Sciences at the Microscale)

Abstract

ABSTRACT Na 2 S, as the terminal discharge product of room‐temperature sodium–sulfur (Na–S) batteries, is electronically and ionically insulating. When it deposits as a compact film on the cathode, the cathode will become passivated, hindering electron transport and inhibiting further sulfur conversion reactions. Existing catalyst strategies promote the formation of Na 2 S thermodynamically by enhancing polysulfide adsorption, but this does not address the kinetics passivation issue. Here, we adopt the exchange current density ( j 0 ) as a kinetic descriptor of the Na 2 S nucleation mode. Finite‐element simulations reveal that increasing j 0 drives the nucleation pathway from progressive to instantaneous nucleation. The deposit morphology then evolves from a compact passivating film to uniformly dispersed nanoparticles, and ion and electron transport channels are preserved. This pathway prevents Na 2 S aggregation and electrode passivation, maintaining electrochemical activity at deep discharge. Guided by this kinetic insight, nitrogen‐doped porous carbon‐supported V single‐atom catalysts (NPC‐V SACs) with high apparent j 0 were fabricated, and instantaneous Na 2 S nucleation was achieved on their surfaces. The resulting Na–S battery retains 976.3 mAh g −1 after 200 cycles at 0.2 A g −1 , with a decay rate of only 0.08% per cycle. This work establishes a kinetic design perspective for regulating Na 2 S nucleation in durable Na–S batteries.

Article Details

Volume / Issue Vol. 1, Issue 1
Published August 06, 2026
ISSN 1433-7851
Publisher Wiley

Journal Info

Angewandte Chemie International Edition

Wiley

ISSN: 1433-7851 Physical Sciences

Authors (17)

G

Guangxuan Wu

School of Energy (National Industry‐Education Platform for Energy Storage) School of Materials Science and Engineering and Tianjin Key Laboratory of Composite and Functional Materials Tianjin University Tianjin People's Republic of China

Z

Zhihui Zhou

State Key Laboratory of Physical Chemistry of Solid Surfaces, Key Laboratory for Chemical Biology of Fujian Province, The MOE Key Laboratory of Spectrochemical Analysis and Instrumentation, Department of Chemical Biology, College of Chemistry and Chemical Engineering, State Key Laboratory of Vaccines for Infectious Diseases, Fujian Provincial Key Laboratory of Innovative Drug Target Research, School of Pharmaceutical Sciences, School of Life Sciences, Faculty of Medicine and Life Sciences

Y

Yeteng Lu

School of Energy (National Industry‐Education Platform for Energy Storage) School of Materials Science and Engineering and Tianjin Key Laboratory of Composite and Functional Materials Tianjin University Tianjin People's Republic of China

Z

Zhoujie Lao

Y

Yuhan Ma

N

Nan Xiao

School of Energy (National Industry‐Education Platform for Energy Storage) School of Materials Science and Engineering and Tianjin Key Laboratory of Composite and Functional Materials Tianjin University Tianjin People's Republic of China

N

Ning Wang

C

Congqin Zheng

Suzhou Nuclear Power Research Institute Jiangsu People's Republic of China

S

Shuiyong Wang

Suzhou Nuclear Power Research Institute Jiangsu People's Republic of China

E

Enzuo Liu

School of Materials Science and Engineering and Tianjin Key Laboratory of Composites and Functional Materials

X

Xiang Zhang

C

Chunsheng Shi

School of Energy (National Industry‐Education Platform for Energy Storage) School of Materials Science and Engineering and Tianjin Key Laboratory of Composite and Functional Materials Tianjin University Tianjin People's Republic of China

C

Chunnian He

W

Wenbin Hu

N

Naiqin Zhao

W

Wanxiang Zhao

Suzhou Nuclear Power Research Institute Jiangsu People's Republic of China

B

Biao Chen

Department of Chemical Physics, School of Chemistry and Materials Science, Hefei National Research Center for Physical Sciences at the Microscale