Hydrogen Aggregation Enhances CO <sub>2</sub> Hydrogenation to Methanol Over In <sub>2</sub> O <sub>3</sub> ‐Based Catalysts

C Chunliang Wang (State Key Laboratory of Complex Nonferrous Metal Resources Clean Utilization School of Metallurgical and Energy Engineering Engineering Research Center of Metallurgical Energy Conservation and Emission Reduction Ministry of Education Kunming University of Science and Technology Kunming Yunnan China) B Beibei Wang D Dong Tian (Pingyuan Laboratory, School of Chemistry and Chemical Engineering) Y Yuhao Wang (Key Laboratory of Biomedical Polymers-Ministry of Education, College of Chemistry and Molecular Sciences) Y Yane Zheng (School of Chemical Engineering Kunming University of Science and Technology Kunming Yunnan China) Y Yuxin Wang (Department of Chemistry) Z Zhi Liu (Laboratory of Atmospheric Environment and Pollution Control) K Kang Cheng H Hua Wang K Kongzhai Li

Abstract

ABSTRACT The hydrogen (H) spillover on the catalyst surface is crucial in the CO 2 hydrogenation reaction, but its effects on product selectivity have been rarely investigated. Herein, we reveal the H‐spillover mediated regulatory role of oxide supports, which changed the CO 2 hydrogenation selectivity on In 2 O 3 ‐based catalysts. By replacing the supports from TiO 2 to ZrO 2 , the primary product of CO 2 hydrogenation experiences a significant shift from carbon monoxide (95.6%) to methanol (84.2%). In situ characterization and theoretical modeling evidence that the degree of H‐spillover influences the distribution of surface hydrogen species on In 2 O 3 ‐based catalysts, affecting the hydrogenation behavior of formate intermediates and the product distribution. The results illustrate the intrinsic relationship between surface hydrogen atom concentration and methanol synthesis rate in catalytic CO 2 hydrogenation over In 2 O 3 ‐based catalysts. This provides the potential to design selective catalysts for CO 2 hydrogenation by modulating the degree of H‐spillover.

Article Details

Volume / Issue Vol. 65, Issue 13
Published March 23, 2026
ISSN 1433-7851
Publisher Wiley

Journal Info

Angewandte Chemie International Edition

Wiley

ISSN: 1433-7851 Physical Sciences

Authors (10)

C

Chunliang Wang

State Key Laboratory of Complex Nonferrous Metal Resources Clean Utilization School of Metallurgical and Energy Engineering Engineering Research Center of Metallurgical Energy Conservation and Emission Reduction Ministry of Education Kunming University of Science and Technology Kunming Yunnan China

B

Beibei Wang

D

Dong Tian

Pingyuan Laboratory, School of Chemistry and Chemical Engineering

Y

Yuhao Wang

Key Laboratory of Biomedical Polymers-Ministry of Education, College of Chemistry and Molecular Sciences

Y

Yane Zheng

School of Chemical Engineering Kunming University of Science and Technology Kunming Yunnan China

Y

Yuxin Wang

Department of Chemistry

Z

Zhi Liu

Laboratory of Atmospheric Environment and Pollution Control

K

Kang Cheng

H

Hua Wang

K

Kongzhai Li