How Does the Precursor Influence the Li‐Rich Layered Oxide Cathode?

Y Yizhen Huang C Chunpu Li (State Key Laboratory of Physical Chemistry of Solid Surfaces, Department of Chemistry, College of Chemistry and Chemical Engineering Xiamen University Xiamen 361005 P. R. China) K Kang Zhang (Qi Biodesign, Beijing, China.) Y Yonglin Tang (State Key Laboratory of Physical Chemistry of Solid Surfaces, Department of Chemistry, College of Chemistry and Chemical Engineering Xiamen University Xiamen 361005 P. R. China) W Wenbin Tu (State Key Laboratory of Physical Chemistry of Solid Surfaces, Department of Chemistry, College of Chemistry and Chemical Engineering Xiamen University Xiamen P. R. China) Y Yuan Tian J Junhao Wang (Beijing National Laboratory for Molecular Sciences (BNLMS), College of Chemistry and Molecular Engineering) Y Yawen Yan (State Key Laboratory of Physical Chemistry of Solid Surfaces, Department of Chemistry, College of Chemistry and Chemical Engineering Xiamen University Xiamen P. R. China) Y Yilong Chen (State Key Laboratory of Physical Chemistry of Solid Surfaces, Collaborative Innovation Center of Chemistry for Energy Materials (iChEM), Department of Chemistry, College of Chemistry and Chemical Engineering) Y Yue Zou L Lianpeng Li (State Key Laboratory of Physical Chemistry of Solid Surfaces, Department of Chemistry, College of Chemistry and Chemical Engineering Xiamen University Xiamen 361005 P. R. China) B Baodan Zhang (Center of Advanced Electrochemical Energy, Institute of Advanced Interdisciplinary Studies, School of Chemistry and Chemical Engineering) J Jun Bao (SINOPEC Research Institute of Petroleum Processing) C Chuxiong Ding (Research Center of R&D Insitute BASF Shanshan Battery Materials Co., Ltd Changsha Hunan 410221 P. R. China) Y Yongchen Wang T Tian Qiu (Department of Chemical and Systems Biology, ChEM-H and Stanford Cancer Institute, Stanford Medical School) X Xin Sun Y Yu Qiao S Shi‐Gang Sun (State Key Laboratory of Physical Chemistry of Solid Surfaces College of Chemistry and Chemical Engineering Xiamen University Xiamen P. R. China)

Abstract

Abstract As a fundamental determinant of Li‐ion battery (LIB) cathode performance and production scalability/feasibility, selection and optimization of precursors represent an essential challenge for the commercialization of layered oxide cathodes. However, for lithium‐rich layered oxide (LRLO) cathodes, the overwhelming majority of laboratory research has rigidly continued to employ carbonate precursors for further modifications while ignoring the potential of hydroxide precursors, which have been undisputedly utilized as commercial precursors for large‐scale production of nickel–cobalt–manganese oxide (NCM) cathodes. This bias toward precursor selection seriously impedes the practical application of the LRLO cathode and largely wastes the resources of lab‐scale scientific research. Herein, through comparative analysis, the structure‐property relationship between carbonate precursor‐derived (CO3‐) and hydroxide precursor‐derived (OH‐) LRLO cathodes was established, elucidating the significance of particle architectural features, especially primary‐particle stacking density (PSD). Specifically, the lower PSD of the CO3‐LRLO cathode facilitates Li⁺ diffusion by enriching the electrolyte‐infiltrated ionic transport pathway but introduces cracks that reduce the volumetric energy density and interfacial/thermal stability. In contrast, the higher PSD of the OH‐LRLO cathode improves structural integrity by enhancing the covalent environment, layered structure, and particle architecture. Moreover, multiple optimization approaches have been proposed and implemented (e.g., electrolyte engineering, lattice doping, and blending strategies) to mitigate inherent drawbacks derived from various precursors.

Article Details

Volume / Issue Vol. 64, Issue 52
Published December 22, 2025
ISSN 1433-7851
Publisher Wiley

Journal Info

Angewandte Chemie International Edition

Wiley

ISSN: 1433-7851 Physical Sciences

Authors (19)

Y

Yizhen Huang

C

Chunpu Li

State Key Laboratory of Physical Chemistry of Solid Surfaces, Department of Chemistry, College of Chemistry and Chemical Engineering Xiamen University Xiamen 361005 P. R. China

K

Kang Zhang

Qi Biodesign, Beijing, China.

Y

Yonglin Tang

State Key Laboratory of Physical Chemistry of Solid Surfaces, Department of Chemistry, College of Chemistry and Chemical Engineering Xiamen University Xiamen 361005 P. R. China

W

Wenbin Tu

State Key Laboratory of Physical Chemistry of Solid Surfaces, Department of Chemistry, College of Chemistry and Chemical Engineering Xiamen University Xiamen P. R. China

Y

Yuan Tian

J

Junhao Wang

Beijing National Laboratory for Molecular Sciences (BNLMS), College of Chemistry and Molecular Engineering

Y

Yawen Yan

State Key Laboratory of Physical Chemistry of Solid Surfaces, Department of Chemistry, College of Chemistry and Chemical Engineering Xiamen University Xiamen P. R. China

Y

Yilong Chen

State Key Laboratory of Physical Chemistry of Solid Surfaces, Collaborative Innovation Center of Chemistry for Energy Materials (iChEM), Department of Chemistry, College of Chemistry and Chemical Engineering

Y

Yue Zou

L

Lianpeng Li

State Key Laboratory of Physical Chemistry of Solid Surfaces, Department of Chemistry, College of Chemistry and Chemical Engineering Xiamen University Xiamen 361005 P. R. China

B

Baodan Zhang

Center of Advanced Electrochemical Energy, Institute of Advanced Interdisciplinary Studies, School of Chemistry and Chemical Engineering

J

Jun Bao

SINOPEC Research Institute of Petroleum Processing

C

Chuxiong Ding

Research Center of R&D Insitute BASF Shanshan Battery Materials Co., Ltd Changsha Hunan 410221 P. R. China

Y

Yongchen Wang

T

Tian Qiu

Department of Chemical and Systems Biology, ChEM-H and Stanford Cancer Institute, Stanford Medical School

X

Xin Sun

Y

Yu Qiao

S

Shi‐Gang Sun

State Key Laboratory of Physical Chemistry of Solid Surfaces College of Chemistry and Chemical Engineering Xiamen University Xiamen P. R. China