From Lignocellulose to Sustainable Aviation Fuel: Innovative Synthesis through Friedel–Crafts Alkylation and Hydrodeoxygenation

H Hannes Latine (Department of Microbial and Molecular Systems (M<sup>2</sup>S) Center for Sustainable Catalysis and Engineering (CSCE) KU Leuven, Faculty of Bioscience Engineering Celestijnenlaan 200F Heverlee 3001 Belgium) D Dario Vangestel (Department of Microbial and Molecular Systems (M<sup>2</sup>S) Center for Sustainable Catalysis and Engineering (CSCE) KU Leuven, Faculty of Bioscience Engineering Celestijnenlaan 200F Heverlee 3001 Belgium) B Bruno Pandalone (Department of Microbial and Molecular Systems (M<sup>2</sup>S) Center for Sustainable Catalysis and Engineering (CSCE) KU Leuven, Faculty of Bioscience Engineering Celestijnenlaan 200F Heverlee 3001 Belgium) D Deepak Raikwar (Department of Microbial and Molecular Systems (M<sup>2</sup>S) Center for Sustainable Catalysis and Engineering (CSCE) KU Leuven, Faculty of Bioscience Engineering Celestijnenlaan 200F Heverlee 3001 Belgium) K Katelijne Lagae (Department of Microbial and Molecular Systems (M<sup>2</sup>S) Center for Sustainable Catalysis and Engineering (CSCE) KU Leuven, Faculty of Bioscience Engineering Celestijnenlaan 200F Heverlee 3001 Belgium) B Bert F. Sels (Center for Sustainable Catalysis and Engineering, KU Leuven, Celestijnenlaan 200F, Leuven 3001, Belgium)

Abstract

Abstract To address the aviation sector's growing carbon footprint, this study presents a novel route for producing sustainable aviation fuel precursors via acid‐catalyzed Friedel–Crafts alkylation of wood‐derived lignin monomers with furfuryl alcohol. Using guaiacol as a model compound, key catalytic requirements were investigated in batch mode. Although heterogeneous zeolites showed initial promise, pore blocking by oligomerized furfuryl alcohol limited performance, leading to the selection of para‐toluenesulfonic acid as an effective homogeneous catalyst. A fed‐batch strategy was employed to suppress oligomerization by controlling furfuryl alcohol concentration. The resulting alkylated products, structurally aligned with conventional kerosene, were further upgraded via metal‐catalyzed hydrodeoxygenation, achieving final overall yields up to 92 C%.

Article Details

Volume / Issue Vol. 64, Issue 49
Published December 01, 2025
ISSN 1433-7851
Publisher Wiley

Journal Info

Angewandte Chemie International Edition

Wiley

ISSN: 1433-7851 Physical Sciences

Authors (6)

H

Hannes Latine

Department of Microbial and Molecular Systems (M<sup>2</sup>S) Center for Sustainable Catalysis and Engineering (CSCE) KU Leuven, Faculty of Bioscience Engineering Celestijnenlaan 200F Heverlee 3001 Belgium

D

Dario Vangestel

Department of Microbial and Molecular Systems (M<sup>2</sup>S) Center for Sustainable Catalysis and Engineering (CSCE) KU Leuven, Faculty of Bioscience Engineering Celestijnenlaan 200F Heverlee 3001 Belgium

B

Bruno Pandalone

Department of Microbial and Molecular Systems (M<sup>2</sup>S) Center for Sustainable Catalysis and Engineering (CSCE) KU Leuven, Faculty of Bioscience Engineering Celestijnenlaan 200F Heverlee 3001 Belgium

D

Deepak Raikwar

Department of Microbial and Molecular Systems (M<sup>2</sup>S) Center for Sustainable Catalysis and Engineering (CSCE) KU Leuven, Faculty of Bioscience Engineering Celestijnenlaan 200F Heverlee 3001 Belgium

K

Katelijne Lagae

Department of Microbial and Molecular Systems (M<sup>2</sup>S) Center for Sustainable Catalysis and Engineering (CSCE) KU Leuven, Faculty of Bioscience Engineering Celestijnenlaan 200F Heverlee 3001 Belgium

B

Bert F. Sels

Center for Sustainable Catalysis and Engineering, KU Leuven, Celestijnenlaan 200F, Leuven 3001, Belgium