Field‐Induced Structural Dynamics of Polarization Switching in Hf <sub>x</sub> Zr <sub>1‐x</sub> O <sub>2</sub> Thin Films

S Sangjun Lee (Department of Biomedical Engineering, University of Minnesota) S Sunghyun Kim S Seong Yong Park D Donghyun Kim S Su Yong Lee (Pohang Light Source‐II (PLS‐II) Beamline Department Pohang Accelerator Laboratory Pohang University of Science and Technology (POSTECH) Pohang 37673 Republic of Korea) D Daseul Ham (Pohang Accelerator Laboratory POSTECH Pohang 37673 Republic of Korea) H Hyun Hwi Lee D Dongjin Yun (Samsung Advanced Institute of Technology (SAIT) Samsung Electronics Co., Ltd Suwon 16678 Republic of Korea) S Seontae Park (Samsung Advanced Institute of Technology (SAIT) Samsung Electronics Co., Ltd Suwon 16678 Republic of Korea) S Soohwan Sul S Seungjin Kang (AI Center Samsung Electronics Co., Ltd Suwon 16678 Republic of Korea) G Geonu Kim (AI Center Samsung Electronics Co., Ltd Suwon 16678 Republic of Korea) D Duk‐Hyun Choe (Samsung Advanced Institute of Technology (SAIT) Samsung Electronics Co., Ltd Suwon 16678 Republic of Korea) J Jooho Lee B Beomseok Kim (Semiconductor R&amp;D Center Samsung Electronics Co., Ltd Hwaseong 18448 Republic of Korea) J Jinseong Heo H Hyung‐Suk Jung (Semiconductor R&amp;D Center Samsung Electronics Co., Ltd Hwaseong 18448 Republic of Korea) H Hanjin Lim (Semiconductor R&amp;D Center Samsung Electronics Co., Ltd Hwaseong 18448 Republic of Korea) W Wonsik Choi (Semiconductor R&amp;D Center Samsung Electronics Co., Ltd Hwaseong 18448 Republic of Korea) J Jeong‐Gyu Song (Samsung Advanced Institute of Technology (SAIT) Samsung Electronics Co., Ltd Suwon 16678 Republic of Korea)

Abstract

Abstract The polarization characteristics of Hf x Zr 1‐x O 2 (HZO) are intrinsically linked to its crystal structure. Optimizing its functionality in ferroelectric (FE) and antiferroelectric (AFE) devices requires understanding the structural evolution during polarization switching, which remains insufficiently understood. Here, the switching mechanism in HZO thin films is elucidated by combining in situ microbeam grazing incidence X‐ray diffraction and first‐principles‐based metadynamics simulations, providing unambiguous evidence of phase evolution. Across compositions ( x = 0 to 0.5), switching involves reversible transitions between the nonpolar tetragonal (t) P 4 2 / nmc and polar orthorhombic (o) Pca 2 1 phases. Zr‐rich AFE compounds undergo a complete t‐phase transition during polarization reversal, while in Hf‐rich FE compounds, transient t‐phase formation facilitates the nucleation and growth of o‐phase domains with reversed polarization. This study promotes engineering phase evolution in HZO for advanced devices.

Article Details

Volume / Issue Vol. 38, Issue 3
Published January 01, 2026
ISSN 0935-9648
Publisher Unknown Publisher

Journal Info

Advanced Materials

Unknown Publisher

ISSN: 0935-9648 Physical Sciences

Authors (20)

S

Sangjun Lee

Department of Biomedical Engineering, University of Minnesota

S

Sunghyun Kim

S

Seong Yong Park

D

Donghyun Kim

S

Su Yong Lee

Pohang Light Source‐II (PLS‐II) Beamline Department Pohang Accelerator Laboratory Pohang University of Science and Technology (POSTECH) Pohang 37673 Republic of Korea

D

Daseul Ham

Pohang Accelerator Laboratory POSTECH Pohang 37673 Republic of Korea

H

Hyun Hwi Lee

D

Dongjin Yun

Samsung Advanced Institute of Technology (SAIT) Samsung Electronics Co., Ltd Suwon 16678 Republic of Korea

S

Seontae Park

Samsung Advanced Institute of Technology (SAIT) Samsung Electronics Co., Ltd Suwon 16678 Republic of Korea

S

Soohwan Sul

S

Seungjin Kang

AI Center Samsung Electronics Co., Ltd Suwon 16678 Republic of Korea

G

Geonu Kim

AI Center Samsung Electronics Co., Ltd Suwon 16678 Republic of Korea

D

Duk‐Hyun Choe

Samsung Advanced Institute of Technology (SAIT) Samsung Electronics Co., Ltd Suwon 16678 Republic of Korea

J

Jooho Lee

B

Beomseok Kim

Semiconductor R&amp;D Center Samsung Electronics Co., Ltd Hwaseong 18448 Republic of Korea

J

Jinseong Heo

H

Hyung‐Suk Jung

Semiconductor R&amp;D Center Samsung Electronics Co., Ltd Hwaseong 18448 Republic of Korea

H

Hanjin Lim

Semiconductor R&amp;D Center Samsung Electronics Co., Ltd Hwaseong 18448 Republic of Korea

W

Wonsik Choi

Semiconductor R&amp;D Center Samsung Electronics Co., Ltd Hwaseong 18448 Republic of Korea

J

Jeong‐Gyu Song

Samsung Advanced Institute of Technology (SAIT) Samsung Electronics Co., Ltd Suwon 16678 Republic of Korea