Elucidating the Correlation Between the Redox Potential, Spin State, and Crystal Structure in a Series of Ferrous Complexes with Redox‐Active Ligands

L Livia Getzner (LCC, CNRS and Université de Toulouse, UPS, INP) Y Yasmine Remili (LCC, CNRS and Université de Toulouse, UPS, INP) Z Zakaria Ziani (LCC: Laboratoire de Chimie de Coordination CNRS France) L Laure Vendier (LCC, CNRS and Université de Toulouse, UPS, INP) W William Nicolazzi (LCC: Laboratoire de Chimie de Coordination CNRS France) A Aurelian Rotaru (Department of Electrical Engineering and Computer Science and MANSiD Research Center, “Stefan Cel Mare” University, University Street, 13, Suceava 720229, Romania) H Haizhu Yu (Department of Chemistry and Centre for Atomic Engineering of Advanced Materials, Key Laboratory of Structure and Functional Regulation of Hybrid Materials of Ministry of Education, Institutes of Physical Science and Information Technology and Anhui Province Key Laboratory of Chemistry for Inorganic/Organic Hybrid Functionalized Materials, Anhui University 1 , Hefei, Anhui 230601,) G Gábor Molnár (LCC, CNRS and Université de Toulouse, UPS, INP) S Saioa Cobo (LCC, CNRS and Université de Toulouse, UPS, INP) A Azzedine Bousseksou (LCC, CNRS and Université de Toulouse, UPS, INP)

Abstract

Abstract Accurately predicting the spin crossover (SCO) temperature ( T 1/2 ) in spin crossover compounds remains a significant challenge due to their extreme sensitivity to minor variations in ligand and crystal structure. In this study, we uncover a critical link between the redox potential of ligands and SCO behavior within Hofmann‐type clathrates {Fe(R‐pbpy⁺)₂[μ₂‐M(CN)₄]₂} (R = electron‐donating or electron‐withdrawing groups, M = Pd or Pt). Through precise tuning of the ligands' electronic properties, we establish a correlation between redox potential, space group, and SCO temperature, explained by an adaptation of Marcus theory of electron transfer. These findings not only provide a deeper understanding of the factors governing SCO behavior but also present a promising strategy for the rational design of SCO materials with tailored properties.

Article Details

Volume / Issue Vol. 64, Issue 32
Published August 04, 2025
ISSN 1433-7851
Publisher Wiley

Journal Info

Angewandte Chemie International Edition

Wiley

ISSN: 1433-7851 Physical Sciences

Authors (10)

L

Livia Getzner

LCC, CNRS and Université de Toulouse, UPS, INP

Y

Yasmine Remili

LCC, CNRS and Université de Toulouse, UPS, INP

Z

Zakaria Ziani

LCC: Laboratoire de Chimie de Coordination CNRS France

L

Laure Vendier

LCC, CNRS and Université de Toulouse, UPS, INP

W

William Nicolazzi

LCC: Laboratoire de Chimie de Coordination CNRS France

A

Aurelian Rotaru

Department of Electrical Engineering and Computer Science and MANSiD Research Center, “Stefan Cel Mare” University, University Street, 13, Suceava 720229, Romania

H

Haizhu Yu

Department of Chemistry and Centre for Atomic Engineering of Advanced Materials, Key Laboratory of Structure and Functional Regulation of Hybrid Materials of Ministry of Education, Institutes of Physical Science and Information Technology and Anhui Province Key Laboratory of Chemistry for Inorganic/Organic Hybrid Functionalized Materials, Anhui University 1 , Hefei, Anhui 230601,

G

Gábor Molnár

LCC, CNRS and Université de Toulouse, UPS, INP

S

Saioa Cobo

LCC, CNRS and Université de Toulouse, UPS, INP

A

Azzedine Bousseksou

LCC, CNRS and Université de Toulouse, UPS, INP