Electrochemistry‐Accelerated Water–Gas Shift Reaction on IrN <sub>4</sub> –RhN <sub>4</sub> Dual Sites Catalysts for Efficient Hydrogen Production

Q Qie Liu (State Key Laboratory of Chemo and Biosensing College of Chemistry and Chemical Engineering International Joint Lab of Energy Electrochemistry of the Ministry of Education Hunan University Changsha 410082 China) L Liyuan Gong (State Key Laboratory of Chemo and Biosensing College of Chemistry and Chemical Engineering International Joint Lab of Energy Electrochemistry of the Ministry of Education Hunan University Changsha 410082 China) J Jingjing Wang L Luyao Ma (State Key Laboratory of Chemo and Biosensing, College of Chemistry and Chemical Engineering) Y Yandong Wu Y Yu‐Cheng Huang (National Synchrotron Radiation Research Center Hsinchu 300092 Taiwan) T Ta Thi Thuy Nga (Research Center for X-ray Science & Department of Physics) Y Yabin Xu (State Key Laboratory of Chemo and Biosensing College of Chemistry and Chemical Engineering International Joint Lab of Energy Electrochemistry of the Ministry of Education Hunan University Changsha 410082 China) Z Zuyao Jiang (State Key Laboratory of Chemo and Biosensing College of Chemistry and Chemical Engineering International Joint Lab of Energy Electrochemistry of the Ministry of Education Hunan University Changsha 410082 China) S Shiqian Du (State Key Laboratory of Chemo and Biosensing College of Chemistry and Chemical Engineering International Joint Lab of Energy Electrochemistry of the Ministry of Education Hunan University Changsha 410082 China) H Hongjing Zhong (State Key Laboratory of Chemo and Biosensing College of Chemistry and Chemical Engineering International Joint Lab of Energy Electrochemistry of the Ministry of Education Hunan University Changsha 410082 China) Y Yanjing Wang M Miaoyu Li C Chung‐Li Dong (Department of Physics Tamkang University New Taipei City Taiwan) G Guobin Wen (State Key Laboratory of Chemo and Biosensing, College of Chemistry and Chemical Engineering) L Li Tao (State Key Laboratory of Chemo and Biosensing, College of Chemistry and Chemical Engineering, Hunan University) S Shuangyin Wang (State Key Laboratory of Chem/Bio-Sensing and Chemometrics, College of Chemistry and Chemical Engineering)

Abstract

Abstract The water–gas shift reaction (WGSR) is crucial to the hydrogen economy, which is hampered by the harsh conditions and complicated purification process. In this work, the spatially separated efficient CO conversion and high‐purity H 2 production are realized by electrochemistry‐accelerated water–gas shift reaction (WGSR) with IrN 4 –RhN 4 dual sites single atom catalysts (IrRh–NC) in high‐temperature polymer–electrolyte–membrane electrolyzer. In this reaction, the Ir single atoms in the catalysts can rapidly dissociate H 2 O at an extremely low potential to supply abundant *OH, which ensures the *OH groups bind to the spontaneously adsorbed *CO on neighboring Rh sites to further accelerate CO conversion. What's more, the elevated temperatures (120–300 °C) maintain water in the gaseous state during the reaction, thus greatly facilitating mass transfer of the reactants CO and H 2 O within the reactor. Employing IrRh–NC as the anodic catalyst, the electrolyzer achieves superior CO catalytic performance (424 mA cm −2 at 0.4 V) and high purity (99.9%) H 2 production (3.2 ml min −1 ), surpassing the performance of particle catalysts. This work illuminates the tantalizing possibility for sustainable hydrogen economic development.

Article Details

Volume / Issue Vol. 64, Issue 44
Published October 27, 2025
ISSN 1433-7851
Publisher Wiley

Journal Info

Angewandte Chemie International Edition

Wiley

ISSN: 1433-7851 Physical Sciences

Authors (17)

Q

Qie Liu

State Key Laboratory of Chemo and Biosensing College of Chemistry and Chemical Engineering International Joint Lab of Energy Electrochemistry of the Ministry of Education Hunan University Changsha 410082 China

L

Liyuan Gong

State Key Laboratory of Chemo and Biosensing College of Chemistry and Chemical Engineering International Joint Lab of Energy Electrochemistry of the Ministry of Education Hunan University Changsha 410082 China

J

Jingjing Wang

L

Luyao Ma

State Key Laboratory of Chemo and Biosensing, College of Chemistry and Chemical Engineering

Y

Yandong Wu

Y

Yu‐Cheng Huang

National Synchrotron Radiation Research Center Hsinchu 300092 Taiwan

T

Ta Thi Thuy Nga

Research Center for X-ray Science & Department of Physics

Y

Yabin Xu

State Key Laboratory of Chemo and Biosensing College of Chemistry and Chemical Engineering International Joint Lab of Energy Electrochemistry of the Ministry of Education Hunan University Changsha 410082 China

Z

Zuyao Jiang

State Key Laboratory of Chemo and Biosensing College of Chemistry and Chemical Engineering International Joint Lab of Energy Electrochemistry of the Ministry of Education Hunan University Changsha 410082 China

S

Shiqian Du

State Key Laboratory of Chemo and Biosensing College of Chemistry and Chemical Engineering International Joint Lab of Energy Electrochemistry of the Ministry of Education Hunan University Changsha 410082 China

H

Hongjing Zhong

State Key Laboratory of Chemo and Biosensing College of Chemistry and Chemical Engineering International Joint Lab of Energy Electrochemistry of the Ministry of Education Hunan University Changsha 410082 China

Y

Yanjing Wang

M

Miaoyu Li

C

Chung‐Li Dong

Department of Physics Tamkang University New Taipei City Taiwan

G

Guobin Wen

State Key Laboratory of Chemo and Biosensing, College of Chemistry and Chemical Engineering

L

Li Tao

State Key Laboratory of Chemo and Biosensing, College of Chemistry and Chemical Engineering, Hunan University

S

Shuangyin Wang

State Key Laboratory of Chem/Bio-Sensing and Chemometrics, College of Chemistry and Chemical Engineering