Electrochemical Conversion of Methane to C <sub>2+</sub> Hydrocarbons and Hydrogen

Y Yige Guo (State Key Laboratory of Catalysis, Dalian National Laboratory for Clean Energy, iChEM (Collaborative Innovation Center of Chemistry for Energy Materials) Dalian Institute of Chemical Physics) T Tianfu Liu (State Key Laboratory of Catalysis, Dalian National Laboratory for Clean Energy, iChEM (Collaborative Innovation Center of Chemistry for Energy Materials) Dalian Institute of Chemical Physics) M Minggao Xu (National Synchrotron Radiation Laboratory) S Shaowei Zhang (State Key Laboratory of Catalysis, Dalian National Laboratory for Clean Energy, iChEM (Collaborative Innovation Center of Chemistry for Energy Materials) Dalian Institute of Chemical Physics) X Xiaomin Zhang (State Key Laboratory of Catalysis, Dalian National Laboratory for Clean Energy, iChEM (Collaborative Innovation Center of Chemistry for Energy Materials)) B Bote Zhao (School of Environment and Energy) L Linjuan Zhang (Key Laboratory of Interfacial Physics and Technology) L Long Zhao (Key Laboratory of Evolution and Marine Biodiversity (Ministry of Education) and Institute of Evolution and Marine Biodiversity, Ocean University of China, Qingdao, China.) Y Yang Pan (National Synchrotron Radiation Laboratory) Y Yuefeng Song (State Key Laboratory of Catalysis, Dalian National Laboratory for Clean Energy, iChEM (Collaborative Innovation Center of Chemistry for Energy Materials) Dalian Institute of Chemical Physics) G Guoxiong Wang (State Key Laboratory of Catalysis, Dalian National Laboratory for Clean Energy, iChEM (Collaborative Innovation Center of Chemistry for Energy Materials) Dalian Institute of Chemical Physics) X Xinhe Bao (State Key Laboratory of Catalysis, Dalian National Laboratory for Clean Energy, iChEM (Collaborative Innovation Center of Chemistry for Energy Materials) Dalian Institute of Chemical Physics)

Abstract

Abstract Catalytic methane (CH 4 ) upgrading to C 2+ products has attracted widespread interest. However, non‐oxidative coupling and oxidative coupling of CH 4 are limited by coking and over‐oxidation, respectively. In this work, we propose an efficient and stable CH 4 conversion system in a solid oxide steam electrolyzer, enabling the simultaneous production of C 2+ hydrocarbons and H 2 . Furthermore, through various in situ characterizations, we reveal a gaseous ·CH 3 radical coupling mechanism underlying the electrochemical CH 4 conversion. These findings pave the way for the efficient design of the electrode for anodic CH 4 coupling reactions in a solid oxide electrolyzer and establish a new framework for atom‐efficient strategies for CH 4 upgrading.

Article Details

Volume / Issue Vol. 64, Issue 42
Published October 13, 2025
ISSN 1433-7851
Publisher Wiley

Journal Info

Angewandte Chemie International Edition

Wiley

ISSN: 1433-7851 Physical Sciences

Authors (12)

Y

Yige Guo

State Key Laboratory of Catalysis, Dalian National Laboratory for Clean Energy, iChEM (Collaborative Innovation Center of Chemistry for Energy Materials) Dalian Institute of Chemical Physics

T

Tianfu Liu

State Key Laboratory of Catalysis, Dalian National Laboratory for Clean Energy, iChEM (Collaborative Innovation Center of Chemistry for Energy Materials) Dalian Institute of Chemical Physics

M

Minggao Xu

National Synchrotron Radiation Laboratory

S

Shaowei Zhang

State Key Laboratory of Catalysis, Dalian National Laboratory for Clean Energy, iChEM (Collaborative Innovation Center of Chemistry for Energy Materials) Dalian Institute of Chemical Physics

X

Xiaomin Zhang

State Key Laboratory of Catalysis, Dalian National Laboratory for Clean Energy, iChEM (Collaborative Innovation Center of Chemistry for Energy Materials)

B

Bote Zhao

School of Environment and Energy

L

Linjuan Zhang

Key Laboratory of Interfacial Physics and Technology

L

Long Zhao

Key Laboratory of Evolution and Marine Biodiversity (Ministry of Education) and Institute of Evolution and Marine Biodiversity, Ocean University of China, Qingdao, China.

Y

Yang Pan

National Synchrotron Radiation Laboratory

Y

Yuefeng Song

State Key Laboratory of Catalysis, Dalian National Laboratory for Clean Energy, iChEM (Collaborative Innovation Center of Chemistry for Energy Materials) Dalian Institute of Chemical Physics

G

Guoxiong Wang

State Key Laboratory of Catalysis, Dalian National Laboratory for Clean Energy, iChEM (Collaborative Innovation Center of Chemistry for Energy Materials) Dalian Institute of Chemical Physics

X

Xinhe Bao

State Key Laboratory of Catalysis, Dalian National Laboratory for Clean Energy, iChEM (Collaborative Innovation Center of Chemistry for Energy Materials) Dalian Institute of Chemical Physics