Dual‐Channel Interdigitated Aptamer‐Based Sensors for Rapid Small‐Molecule Detection in Biofluids

S Senyao Wang A Ali Elmorsy (Laboratory of Chemical Nanotechnology (CHEMINA) École Polytechnique Fédérale de Lausanne (EPFL) Geneva Switzerland) D Defne Tüzün (Neuroelectronics, Munich Institute of Biomedical Engineering Department of Electrical Engineering TUM School of Computation, Information and Technology Technical University of Munich Garching Germany) L Lilly Schmidt (Neuroelectronics, Munich Institute of Biomedical Engineering Department of Electrical Engineering TUM School of Computation, Information and Technology Technical University of Munich Garching Germany) S Sebastian Freko (Neuroelectronics, Munich Institute of Biomedical Engineering Department of Electrical Engineering TUM School of Computation, Information and Technology Technical University of Munich Garching Germany) L Lukas Hiendlmeier (Neuroelectronics, Munich Institute of Biomedical Engineering Department of Electrical Engineering TUM School of Computation, Information and Technology Technical University of Munich Garching Germany) C Chen Wang A Alonso Ingar Romero (Neuroelectronics, Munich Institute of Biomedical Engineering Department of Electrical Engineering TUM School of Computation, Information and Technology Technical University of Munich Garching Germany) G George Al Boustani (Neuroelectronics, Munich Institute of Biomedical Engineering Department of Electrical Engineering TUM School of Computation, Information and Technology Technical University of Munich Garching Germany) H Hu Peng B Berna Özkale (Microrobotic Bioengineering Lab Department of Electrical Engineering TUM School of Computation, Information and Technology Technical University of Munich Garching Germany) N Nako Nakatsuka (Laboratory of Chemical Nanotechnology (CHEMINA) École Polytechnique Fédérale de Lausanne (EPFL) Geneva Switzerland) B Bernhard Wolfrum (Neuroelectronics, Munich Institute of Biomedical Engineering Department of Electrical Engineering TUM School of Computation, Information and Technology Technical University of Munich Garching Germany)

Abstract

ABSTRACT Timely and decentralized quantification of small‐molecule biomarkers is essential for point‐of‐care (POC) diagnostics, but their reliable detection in biofluids remains challenging. Here, we introduce an engineered electrochemical aptamer sensing platform that employs a dual‐channel signal conversion strategy to overcome these limitations. By integrating spatially separated interdigitated working electrodes with selective self‐assembled monolayer (SAM) removal, the system enables target‐induced release and recapture of methylene blue‐labeled complementary DNA (MB‐cDNA) probes across two electrodes. This configuration minimizes background interference and enhances mass transport, facilitating robust dual‐channel signal transduction. The platform enables rapid (≤ 30 min), low‐volume (30 µL) detection of prototypical small molecules, dopamine and cortisol, in diverse biofluids, including artificial cerebrospinal fluid (aCSF), human serum, and saliva. Notably, the signal conversion mechanism remained effective across different targets and sample types, requiring only minimal adaptation of the recognition sequence. Together, these features establish a versatile electrochemical sensing architecture with broad potential for rapid, quantitative small‐molecule analysis in complex biological media.

Article Details

Volume / Issue Vol. 65, Issue 27
Published July 01, 2026
ISSN 1433-7851
Publisher Wiley

Journal Info

Angewandte Chemie International Edition

Wiley

ISSN: 1433-7851 Physical Sciences

Authors (13)

S

Senyao Wang

A

Ali Elmorsy

Laboratory of Chemical Nanotechnology (CHEMINA) École Polytechnique Fédérale de Lausanne (EPFL) Geneva Switzerland

D

Defne Tüzün

Neuroelectronics, Munich Institute of Biomedical Engineering Department of Electrical Engineering TUM School of Computation, Information and Technology Technical University of Munich Garching Germany

L

Lilly Schmidt

Neuroelectronics, Munich Institute of Biomedical Engineering Department of Electrical Engineering TUM School of Computation, Information and Technology Technical University of Munich Garching Germany

S

Sebastian Freko

Neuroelectronics, Munich Institute of Biomedical Engineering Department of Electrical Engineering TUM School of Computation, Information and Technology Technical University of Munich Garching Germany

L

Lukas Hiendlmeier

Neuroelectronics, Munich Institute of Biomedical Engineering Department of Electrical Engineering TUM School of Computation, Information and Technology Technical University of Munich Garching Germany

C

Chen Wang

A

Alonso Ingar Romero

Neuroelectronics, Munich Institute of Biomedical Engineering Department of Electrical Engineering TUM School of Computation, Information and Technology Technical University of Munich Garching Germany

G

George Al Boustani

Neuroelectronics, Munich Institute of Biomedical Engineering Department of Electrical Engineering TUM School of Computation, Information and Technology Technical University of Munich Garching Germany

H

Hu Peng

B

Berna Özkale

Microrobotic Bioengineering Lab Department of Electrical Engineering TUM School of Computation, Information and Technology Technical University of Munich Garching Germany

N

Nako Nakatsuka

Laboratory of Chemical Nanotechnology (CHEMINA) École Polytechnique Fédérale de Lausanne (EPFL) Geneva Switzerland

B

Bernhard Wolfrum

Neuroelectronics, Munich Institute of Biomedical Engineering Department of Electrical Engineering TUM School of Computation, Information and Technology Technical University of Munich Garching Germany