Direct observation of ultrafast symmetry reduction during internal conversion of 2-thiouracil using Coulomb explosion imaging

T Till Jahnke (European XFEL) S Sebastian Mai (Institute of Theoretical Chemistry, Faculty of Chemistry, University of Vienna , Währinger Straße 17, 1090 Vienna,) S Surjendu Bhattacharyya (Stanford PULSE Institute) K Keyu Chen (School of Materials Science and Engineering, State Key Laboratory of Fine Chemicals, Frontiers Science Center for Smart Materials Oriented Chemical Engineering, Technology Innovation Center of High Performance Resin Materials (Liaoning Province)) R Rebecca Boll (European XFEL , Holzkoppel 4 , ,) M Maria Elena Castellani S Simon Dold (European XFEL , Holzkoppel 4 , ,) U Ulrike Frühling A Alice E. Green (EaStCHEM School of Chemistry) M Markus Ilchen (Deutsches Elektronen-Synchrotron DESY , Notkestr. 85 , ,) R Rebecca Ingle G Gregor Kastirke (Institut für Kernphysik) H Huynh Van Sa Lam (James R. Macdonald Laboratory, Physics Department) F Fabiano Lever (Institut für Physik und Astronomie) D Dennis Mayer (Deutsches Elektronen-Synchrotron DESY 2 , 22607 Hamburg,) T Tommaso Mazza T Terence Mullins (European XFEL, Holzkoppel 4, Schenefeld 22869, Germany) Y Yevheniy Ovcharenko B Björn Senfftleben (European XFEL, Holzkoppel 4, Schenefeld 22869, Germany) F Florian Trinter (Fritz-Haber-Institut der Max-Planck-Gesellschaft , , Faradayweg 4-6 , ,) A Atia-Tul-Noor S Sergey Usenko A Anbu Selvam Venkatachalam (James R. Macdonald Laboratory, Physics Department) A Artem Rudenko (James R. Macdonald Laboratory, Physics Department) D Daniel Rolles (James R. Macdonald Laboratory, Physics Department) M Michael Meyer H Heide Ibrahim M Markus Gühr (Institut für Physik und Astronomie)

Abstract

Abstract The photochemistry of heterocyclic molecules plays a decisive role for processes and applications like DNA photo-protection from UV damage and organic photocatalysis. The photochemical reactivity of heterocycles is determined by the redistribution of photoenergy into electronic and nuclear degrees of freedom, initially involving ultrafast internal conversion. Most heterocycles are planar in their ground state and internal conversion requires symmetry breaking. To lower the symmetry, the molecule must undergo an out-of-plane motion, which has not yet been observed directly. Here we show using the example of 2-thiouracil, how Coulomb explosion imaging can be utilized to extract comprehensive information on this molecular deformation, linking the extracted deplanarization of the molecular geometry to the previously studied temporal evolution of its electronic properties. Particularly, the protons of the exploded molecule are well-suited messengers carrying rich information on its geometry at distinct times after electronic excitation. We expect that our new analysis approach centered on these peripheral protons can be adapted as a general concept for future time-resolved studies of complex molecules in the gas phase.

Article Details

Volume / Issue Vol. 16, Issue 1
Published February 28, 2025
ISSN 2041-1723
Publisher Nature Portfolio

Journal Info

Nature Communications

Nature Portfolio

ISSN: 2041-1723 Open Access Life Sciences

Authors (28)

T

Till Jahnke

European XFEL

S

Sebastian Mai

Institute of Theoretical Chemistry, Faculty of Chemistry, University of Vienna , Währinger Straße 17, 1090 Vienna,

S

Surjendu Bhattacharyya

Stanford PULSE Institute

K

Keyu Chen

School of Materials Science and Engineering, State Key Laboratory of Fine Chemicals, Frontiers Science Center for Smart Materials Oriented Chemical Engineering, Technology Innovation Center of High Performance Resin Materials (Liaoning Province)

R

Rebecca Boll

European XFEL , Holzkoppel 4 , ,

M

Maria Elena Castellani

S

Simon Dold

European XFEL , Holzkoppel 4 , ,

U

Ulrike Frühling

A

Alice E. Green

EaStCHEM School of Chemistry

M

Markus Ilchen

Deutsches Elektronen-Synchrotron DESY , Notkestr. 85 , ,

R

Rebecca Ingle

G

Gregor Kastirke

Institut für Kernphysik

H

Huynh Van Sa Lam

James R. Macdonald Laboratory, Physics Department

F

Fabiano Lever

Institut für Physik und Astronomie

D

Dennis Mayer

Deutsches Elektronen-Synchrotron DESY 2 , 22607 Hamburg,

T

Tommaso Mazza

T

Terence Mullins

European XFEL, Holzkoppel 4, Schenefeld 22869, Germany

Y

Yevheniy Ovcharenko

B

Björn Senfftleben

European XFEL, Holzkoppel 4, Schenefeld 22869, Germany

F

Florian Trinter

Fritz-Haber-Institut der Max-Planck-Gesellschaft , , Faradayweg 4-6 , ,

A

Atia-Tul-Noor

S

Sergey Usenko

A

Anbu Selvam Venkatachalam

James R. Macdonald Laboratory, Physics Department

A

Artem Rudenko

James R. Macdonald Laboratory, Physics Department

D

Daniel Rolles

James R. Macdonald Laboratory, Physics Department

M

Michael Meyer

H

Heide Ibrahim

M

Markus Gühr

Institut für Physik und Astronomie