Cyclic Trinuclear Units Based Covalent Metal‐Organic Frameworks for Gold Recovery

J Jie Luo J Jia‐Tong Lin (College of Chemistry and Materials Science Guangdong Provincial Key Laboratory of Supramolecular Coordination Chemistry Jinan University Guangzhou 510632 China) X Xiao Luo N Na Yin M Mo Xie (State Key Laboratory for Flexible Electronics (LoFE)) X Xu Chen (Jinan University , , , ,) Y Ying‐Qiang Li (College of Chemistry and Materials Science Guangdong Provincial Key Laboratory of Supramolecular Coordination Chemistry Jinan University Guangzhou 510632 China) Y Yang‐Guang Li (College of Chemistry and Materials Science Guangdong Provincial Key Laboratory of Supramolecular Coordination Chemistry Jinan University Guangzhou 510632 China) G Guo‐Hong Ning (College of Chemistry and Materials Science Guangdong Provincial Key Laboratory of Supramolecular Coordination Chemistry Jinan University Guangzhou China) D Dan Li

Abstract

Abstract The development of porous solids for gold recovery is highly desired from both an economical and environmental point of view; however, the design of solid adsorbents with high overall performance is still challenging. Herein, we designed three copper(I) cyclic trinuclear units, Cu(I)‐CTUs, based covalent metal‐organic frameworks (CMOFs) by networking metal clusters with dynamic covalent linkages. These CMOFs deliver a high gold adsorption capacity of 3687 mg g −1 , ultra‐fast adsorption kinetics (i.e., removal efficiency > 99% within   20 s), excellent selectivity and reusability. In addition, they can be readily used for gold extraction from e‐waste. Owing to the rich redox properties of Cu‐CTUs, these CMOFs show three sorption mechanisms including adsorption, chemical reduction and photocatalytic reduction. Interestingly, the gold‐loaded CMOFs can be used as catalysts for hydration of alkynes to ketones with high yields (e.g., up to ∼ 95% for 6 examples).

Article Details

Volume / Issue Vol. 64, Issue 27
Published July 01, 2025
ISSN 1433-7851
Publisher Wiley

Journal Info

Angewandte Chemie International Edition

Wiley

ISSN: 1433-7851 Physical Sciences

Authors (10)

J

Jie Luo

J

Jia‐Tong Lin

College of Chemistry and Materials Science Guangdong Provincial Key Laboratory of Supramolecular Coordination Chemistry Jinan University Guangzhou 510632 China

X

Xiao Luo

N

Na Yin

M

Mo Xie

State Key Laboratory for Flexible Electronics (LoFE)

X

Xu Chen

Jinan University , , , ,

Y

Ying‐Qiang Li

College of Chemistry and Materials Science Guangdong Provincial Key Laboratory of Supramolecular Coordination Chemistry Jinan University Guangzhou 510632 China

Y

Yang‐Guang Li

College of Chemistry and Materials Science Guangdong Provincial Key Laboratory of Supramolecular Coordination Chemistry Jinan University Guangzhou 510632 China

G

Guo‐Hong Ning

College of Chemistry and Materials Science Guangdong Provincial Key Laboratory of Supramolecular Coordination Chemistry Jinan University Guangzhou China

D

Dan Li