COFs on MOFs: Layer‐by‐Layer Synthesis of MOF@COF Nanoparticles with Synergistic Adsorption

A Ana Guillem‐Navajas (Departamento de Química Inorgánica Universidad Autónoma de Madrid Madrid 28049 Spain) L Lucía Torrico‐García‐Viso (Departamento de Química Inorgánica Universidad Autónoma de Madrid Madrid 28049 Spain) J Jose Antonio Suárez del Pino (Catalan Institute of Nanoscience and Nanotechnology (ICN2) Campus UAB, Bellaterra Barcelona 08193 Spain) N Nekane Aramburu‐Merino (Departamento de Física de la Materia Condensada Universidad Autónoma de Madrid Madrid 28049 Spain) P Pilar Segovia E Enrique G. Michel (Departamento de Física de la Materia Condensada Universidad Autónoma de Madrid Madrid 28049 Spain) J Josep Puigmartí‐Luis (Departament de Ciència de Materials i Química Física Universitat de Barcelona C/ Martí i Franquès, 1–11 Barcelona 08028 Spain) E Enrique Velasco (Condensed Matter Physics Center (IFIMAC) Universidad Autónoma de Madrid Madrid 28049 Spain) P Pedro Tarazona (Departamento de Física Teórica de la Materia Condensada) D Daniel Maspoch (Catalan Institute of Nanoscience and Nanotechnology (ICN2), CSIC, and The Barcelona Institute of Science and Technology) D David Rodríguez‐San‐Miguel (Departamento de Química Inorgánica Universidad Autónoma de Madrid Madrid 28049 Spain) F Félix Zamora (Departamento de Química Inorgánica, Universidad Autónoma de Madrid)

Abstract

Abstract Synergistic effects between porous materials offer a powerful route to enhance key functionalities such as adsorption, catalysis, and molecular transport. In this context, the combination of metal–organic frameworks (MOFs) and covalent organic frameworks (COFs) provides a promising platform for engineering hybrid adsorbents with synergistic sorption behavior. Here, a versatile layer‐by‐layer strategy is presented for the controlled growth of crystalline COF shells on MOF nanoparticles, yielding uniform MOF@COF nanocomposites as stable aqueous colloids. This approach enables precise tuning of shell thickness and porosity under mild conditions. The resulting core–shell hybrids exhibit enhanced water adsorption, driven by the formation of interfacial mesopores. Modeling studies indicate that a minimum number of COF growth cycles is necessary to induce these mesopores, which interconnect with the intrinsic micropores of the COF shell and facilitate synergistic uptake. This work presents a scalable and modular approach to creating porous hybrid nanoparticles with programmable interfacial architectures and enhanced sorption performance.

Article Details

Volume / Issue Vol. 1, Issue 1
Published November 19, 2025
ISSN 0935-9648
Publisher Unknown Publisher

Journal Info

Advanced Materials

Unknown Publisher

ISSN: 0935-9648 Physical Sciences

Authors (12)

A

Ana Guillem‐Navajas

Departamento de Química Inorgánica Universidad Autónoma de Madrid Madrid 28049 Spain

L

Lucía Torrico‐García‐Viso

Departamento de Química Inorgánica Universidad Autónoma de Madrid Madrid 28049 Spain

J

Jose Antonio Suárez del Pino

Catalan Institute of Nanoscience and Nanotechnology (ICN2) Campus UAB, Bellaterra Barcelona 08193 Spain

N

Nekane Aramburu‐Merino

Departamento de Física de la Materia Condensada Universidad Autónoma de Madrid Madrid 28049 Spain

P

Pilar Segovia

E

Enrique G. Michel

Departamento de Física de la Materia Condensada Universidad Autónoma de Madrid Madrid 28049 Spain

J

Josep Puigmartí‐Luis

Departament de Ciència de Materials i Química Física Universitat de Barcelona C/ Martí i Franquès, 1–11 Barcelona 08028 Spain

E

Enrique Velasco

Condensed Matter Physics Center (IFIMAC) Universidad Autónoma de Madrid Madrid 28049 Spain

P

Pedro Tarazona

Departamento de Física Teórica de la Materia Condensada

D

Daniel Maspoch

Catalan Institute of Nanoscience and Nanotechnology (ICN2), CSIC, and The Barcelona Institute of Science and Technology

D

David Rodríguez‐San‐Miguel

Departamento de Química Inorgánica Universidad Autónoma de Madrid Madrid 28049 Spain

F

Félix Zamora

Departamento de Química Inorgánica, Universidad Autónoma de Madrid