Biomimetic Gradient‐Porous Carbon Enables Sustainable High‐Loading Lithium–Sulfur Batteries by Regulating Polysulfide Chemistry

Z Zihai Cheng (Division of Energy Conversion & Storage, Hefei National Research Center for Physical Sciences at the Microscale, School of Chemistry and Materials Science, CAS Key Laboratory of Mechanical Behavior and Design of Materials (LMBD), School of Engineering Science University of Science and Technology of China Hefei Anhui China) P Ping Wu (Department of Neurobiology, University of Texas Medical Branch) W Wei‐Xu Dong (Division of Energy Conversion & Storage, Hefei National Research Center for Physical Sciences at the Microscale, School of Chemistry and Materials Science, CAS Key Laboratory of Mechanical Behavior and Design of Materials (LMBD), School of Engineering Science University of Science and Technology of China Hefei Anhui China) Z Ze‐Peng Liu (Division of Energy Conversion & Storage, Hefei National Research Center for Physical Sciences at the Microscale, School of Chemistry and Materials Science, CAS Key Laboratory of Mechanical Behavior and Design of Materials (LMBD), School of Engineering Science University of Science and Technology of China Hefei Anhui China) R Rong‐Hao Wang (School of Engineering Science Division of Nanomaterials & Chemistry Hefei National Research Center for Physical Sciences at the Microscale School of Chemistry and Materials Science CAS Key Laboratory of Mechanical Behavior and Design of Materials (LMBD) University of Science and Technology of China Hefei Anhui People's Republic of China) T Tingyu Zhang H Haibo Hu W Wujun Liu (State Key Laboratory of Advanced Environmental Technology Department of Environmental Science and Engineering University of Science and Technology of China Hefei Anhui China) L Li‐Feng Chen (School of Engineering Science Division of Nanomaterials & Chemistry Hefei National Research Center for Physical Sciences at the Microscale School of Chemistry and Materials Science CAS Key Laboratory of Mechanical Behavior and Design of Materials (LMBD) University of Science and Technology of China Hefei Anhui People's Republic of China)

Abstract

ABSTRACT To realize the commercial viability of lithium–sulfur (Li–S) batteries, it is imperative to substantially increase the areal sulfur loading of the cathode to achieve higher energy density. However, increasing sulfur loading inevitably deteriorates charge‐transport efficiency and slows electrochemical reaction kinetics, leading to pronounced degradation in rate capability and cycling stability. To address these critical challenges, a biomimetic strategy is adopted to engineer gradient‐porous nitrogen‐doped carbon nanomaterials (Bio‐N‐CNTs) with radially graded pore architectures, enabling their use as highly effective sulfur host materials. In situ Raman spectroscopy and DFT reveal that such unique structures facilitate efficient mass transport, ion diffusion, sulfur conversion, and high sulfur loading simultaneously, as well as enable gradient confinement catalytic conversion of LiPSs. As a result, the Bio‐N‐CNT/S cathode exhibits a capacity decay rate of only 0.178% after 100 cycles at a 0.1 C rate. Even under high sulfur loading conditions of 8.6 mg cm −2 , this cathode material maintains 71% capacity retention after 100 cycles. Additionally, a sustainable “precipitation‐enrichment‐reduction‐regeneration” silver recovery strategy with a 93% recovery rate, enhancing economic feasibility. This work demonstrates an innovative, scalable, and sustainable biomimetic Bio‐N‐CNT host for practical Li–S batteries.

Article Details

Volume / Issue Vol. 65, Issue 22
Published May 25, 2026
ISSN 1433-7851
Publisher Wiley

Journal Info

Angewandte Chemie International Edition

Wiley

ISSN: 1433-7851 Physical Sciences

Authors (9)

Z

Zihai Cheng

Division of Energy Conversion & Storage, Hefei National Research Center for Physical Sciences at the Microscale, School of Chemistry and Materials Science, CAS Key Laboratory of Mechanical Behavior and Design of Materials (LMBD), School of Engineering Science University of Science and Technology of China Hefei Anhui China

P

Ping Wu

Department of Neurobiology, University of Texas Medical Branch

W

Wei‐Xu Dong

Division of Energy Conversion & Storage, Hefei National Research Center for Physical Sciences at the Microscale, School of Chemistry and Materials Science, CAS Key Laboratory of Mechanical Behavior and Design of Materials (LMBD), School of Engineering Science University of Science and Technology of China Hefei Anhui China

Z

Ze‐Peng Liu

Division of Energy Conversion & Storage, Hefei National Research Center for Physical Sciences at the Microscale, School of Chemistry and Materials Science, CAS Key Laboratory of Mechanical Behavior and Design of Materials (LMBD), School of Engineering Science University of Science and Technology of China Hefei Anhui China

R

Rong‐Hao Wang

School of Engineering Science Division of Nanomaterials & Chemistry Hefei National Research Center for Physical Sciences at the Microscale School of Chemistry and Materials Science CAS Key Laboratory of Mechanical Behavior and Design of Materials (LMBD) University of Science and Technology of China Hefei Anhui People's Republic of China

T

Tingyu Zhang

H

Haibo Hu

W

Wujun Liu

State Key Laboratory of Advanced Environmental Technology Department of Environmental Science and Engineering University of Science and Technology of China Hefei Anhui China

L

Li‐Feng Chen

School of Engineering Science Division of Nanomaterials & Chemistry Hefei National Research Center for Physical Sciences at the Microscale School of Chemistry and Materials Science CAS Key Laboratory of Mechanical Behavior and Design of Materials (LMBD) University of Science and Technology of China Hefei Anhui People's Republic of China