Biomarker‐Gated Photocatalysis Uncaging in Live System

G Guoming Tong (Key Laboratory of Chemical Biology & Traditional Chinese Medicine Research of Ministry of Education, Key Laboratory of Phytochemical R&D of Hunan Province, College of Chemistry and Chemical Engineering Hunan Normal University Changsha Hunan 410081 China) C Changfeng Li (Key Laboratory of Chemical Biology & Traditional Chinese Medicine Research, Ministry of Education, Institute of Interdisciplinary Studies, College of Chemistry and Chemical Engineering) Q Qing Zhou F Fang Wang W Wei He E Erhu Xiong (Key Laboratory of Chemical Biology & Traditional Chinese Medicine Research, Ministry of Education, Institute of Interdisciplinary Studies, College of Chemistry and Chemical Engineering) L Lebin Su S Sheng Yang (Key Laboratory of Chemical Biology & Traditional Chinese Medicine Research, Ministry of Education, Institute of Interdisciplinary Studies, College of Chemistry and Chemical Engineering) G Guhuan Liu (State Key Laboratory of Precision and Intelligent Chemistry, Department of Polymer Science and Engineering, School of Chemistry and Materials Science) R Ronghua Yang (Key Laboratory of Chemical Biology & Traditional Chinese Medicine Research, Ministry of Education, Institute of Interdisciplinary Studies, College of Chemistry and Chemical Engineering)

Abstract

Abstract Spatiotemporal precision in photocontrolled biochemical reactions remains a central challenge. We report a sequential activation platform that integrates biomarker‐triggered unlocking of photocatalyst activity with photocatalytic bioorthogonal uncaging, designed to enhance bioimaging and enable AND‐gate therapeutics. By engineering diiodo‐BODIPY carboxylic acid—an organic photocatalyst enabling efficient azide‐to‐amine reduction under light—we masked its carboxyl group as an ester to completely suppress photocatalytic activity. Strategic incorporation of enzyme‐ or ROS‐cleavable self‐immolative linkers restored catalysis in response to nitroreductase (NTR) or H 2 O 2 , respectively. This “lock‐and‐key” mechanism enables two primary functionalities: enhanced bioimaging through signal amplification by biomarker‐activated BODIPY catalysts, and an “AND‐gate” therapeutic activation requiring both NTR presence and light exposure for the release of caged therapeutic agents like RNase A or doxorubicin. Our platform integrates bioresponsive chemistry with light‐mediated control, offering a blueprint for logical gate‐regulated cellular processes and advancing precision medicine with potential for more targeted and efficient therapies.

Article Details

Volume / Issue Vol. 65, Issue 4
Published January 22, 2026
ISSN 1433-7851
Publisher Wiley

Journal Info

Angewandte Chemie International Edition

Wiley

ISSN: 1433-7851 Physical Sciences

Authors (10)

G

Guoming Tong

Key Laboratory of Chemical Biology & Traditional Chinese Medicine Research of Ministry of Education, Key Laboratory of Phytochemical R&D of Hunan Province, College of Chemistry and Chemical Engineering Hunan Normal University Changsha Hunan 410081 China

C

Changfeng Li

Key Laboratory of Chemical Biology & Traditional Chinese Medicine Research, Ministry of Education, Institute of Interdisciplinary Studies, College of Chemistry and Chemical Engineering

Q

Qing Zhou

F

Fang Wang

W

Wei He

E

Erhu Xiong

Key Laboratory of Chemical Biology & Traditional Chinese Medicine Research, Ministry of Education, Institute of Interdisciplinary Studies, College of Chemistry and Chemical Engineering

L

Lebin Su

S

Sheng Yang

Key Laboratory of Chemical Biology & Traditional Chinese Medicine Research, Ministry of Education, Institute of Interdisciplinary Studies, College of Chemistry and Chemical Engineering

G

Guhuan Liu

State Key Laboratory of Precision and Intelligent Chemistry, Department of Polymer Science and Engineering, School of Chemistry and Materials Science

R

Ronghua Yang

Key Laboratory of Chemical Biology & Traditional Chinese Medicine Research, Ministry of Education, Institute of Interdisciplinary Studies, College of Chemistry and Chemical Engineering