Beyond Electronic Interaction: Ru Sub‐Nanoparticles Reconfiguring Interfacial Water on Ru–Co Diatomic Sites for Accelerated Oxygen Reduction

X Xiangrong Jin (State Key Laboratory of Chemical Resource Engineering, College of Chemistry, Beijing University of Chemical Technology, Beijing 100029, China) Y Yafei Liu (State Key Laboratory of Chemical Resource Engineering, College of Chemistry, Beijing University of Chemical Technology, Beijing 100029, China) H Hao Sun Y Yu Zhang (Xiangya Hospital, Central South University Changsha China) X Xiaoyan Huang Q Qingyi Zhu (Department of Chemistry) K Keying Tao (State Key Laboratory of Chemical Resource Engineering College of Chemistry Beijing University of Chemical Technology Beijing China) Y Yuan Zhang H HaoCheng Wang Y Yuyang Zhou H Hao Song Y Yifan Zeng (State Key Laboratory of Chemical Resource Engineering College of Chemistry Beijing University of Chemical Technology Beijing China) Z Zheng Chang (State Key Laboratory of Chemical Resource Engineering, College of Chemistry, Beijing University of Chemical Technology, Beijing 100029, China) Y Yi Zhao (State Key Laboratory of Quantum Functional Materials, School of Physical Science and Technology) W Wei Zhu C Chang Chen H Hua Zhang N Nana Wang J Jiazhan Li (State Key Laboratory of Chemical Resource Engineering, College of Chemistry, Beijing University of Chemical Technology, Beijing 100029, China) X Xiaoming Sun

Abstract

ABSTRACT Synergy between metallic nanoparticles and single‐atom sites offers considerable potential for developing advanced electrocatalysts. However, the synergistic mechanism in such complex architectures under operating conditions remains elusive. Herein, a two‐step approach involving selective etching and co‐confined adsorption was developed to precisely construct CoRu/Ru NPs catalyst, featuring Ru–Co diatomic sites coupled with Ru sub‐nanoparticles, which demonstrates excellent oxygen reduction reaction (ORR) performance with a half‐wave potential of 0.91 V and a peak power density of 369 mW cm −2 in zinc‐air batteries, along with outstanding cycling stability over 1350 h. Beyond modulating the electronic structure to weaken OH* adsorption on Ru–Co diatomic sites, the Ru sub‐nanoparticles also induce an alternative thermodynamic pathway for enhanced ORR kinetics, in which interfacial water dissociate on oxyphilic Ru sub‐nanoparticles and facilely supply protons to oxygen‐containing intermediates on neighboring Ru–Co diatomic sites. This work not only advances the construction of synergistic active sites but also opens a new paradigm for designing advanced electrocatalysts by harnessing the interfacial environment beyond electronic structure modulation.

Article Details

Volume / Issue Vol. 65, Issue 20
Published May 11, 2026
ISSN 1433-7851
Publisher Wiley

Journal Info

Angewandte Chemie International Edition

Wiley

ISSN: 1433-7851 Physical Sciences

Authors (20)

X

Xiangrong Jin

State Key Laboratory of Chemical Resource Engineering, College of Chemistry, Beijing University of Chemical Technology, Beijing 100029, China

Y

Yafei Liu

State Key Laboratory of Chemical Resource Engineering, College of Chemistry, Beijing University of Chemical Technology, Beijing 100029, China

H

Hao Sun

Y

Yu Zhang

Xiangya Hospital, Central South University Changsha China

X

Xiaoyan Huang

Q

Qingyi Zhu

Department of Chemistry

K

Keying Tao

State Key Laboratory of Chemical Resource Engineering College of Chemistry Beijing University of Chemical Technology Beijing China

Y

Yuan Zhang

H

HaoCheng Wang

Y

Yuyang Zhou

H

Hao Song

Y

Yifan Zeng

State Key Laboratory of Chemical Resource Engineering College of Chemistry Beijing University of Chemical Technology Beijing China

Z

Zheng Chang

State Key Laboratory of Chemical Resource Engineering, College of Chemistry, Beijing University of Chemical Technology, Beijing 100029, China

Y

Yi Zhao

State Key Laboratory of Quantum Functional Materials, School of Physical Science and Technology

W

Wei Zhu

C

Chang Chen

H

Hua Zhang

N

Nana Wang

J

Jiazhan Li

State Key Laboratory of Chemical Resource Engineering, College of Chemistry, Beijing University of Chemical Technology, Beijing 100029, China

X

Xiaoming Sun