Atomic‐Precision Triple‐Enzyme Nanozyme Synchronizes Mitochondrial Dual‐Pathway Disruption for Precision Oncology

Y Yufan Zhang (Key Laboratory of Photochemistry, Research/Education Center for Excellence in Molecular Sciences, Institute of Chemistry, Chinese Academy of Sciences) S Shuangshuang Yang Q Qin Xiang (Marshall Laboratory of Biomedical Engineering, Precision Medicine and Health Research Institute, Shenzhen Key Laboratory for Nano-Biosensing Technology, Guangdong Key Laboratory of Biomedical Measurements and Ultrasound Imaging, School of Biomedical Engineering, Shenzhen University Medical School) J Jinkun Huang (Marshall Laboratory of Biomedical Engineering, Precision Medicine and Health Research Institute, Shenzhen Key Laboratory for Nano-Biosensing Technology, Guangdong Key Laboratory of Biomedical Measurements and Ultrasound Imaging, School of Biomedical Engineering, Shenzhen University Medical School) Y Yongfeng Tan (Marshall Laboratory of Biomedical Engineering, Research Center for Biosensor and Nanotheranostic, School of Biomedical Engineering, Health Science Center Shenzhen University Guangdong 518060 P.R. China) X Xiang Peng (Department of Neurobiology, School of Basic Medicine, Tongji Medical College, Huazhong University of Science and Technology) Y Youming Feng (State Key Laboratory of Analytical Chemistry for Life Science, School of Chemistry and Chemical Engineering Nanjing University Nanjing 210023 P.R. China) R Ran Chang J Jinze Li (CAS Key Lab of Bio-Medical Diagnostics) Y Yaru Cheng (Marshall Laboratory of Biomedical Engineering, Research Center for Biosensor and Nanotheranostic, School of Biomedical Engineering, Health Science Center Shenzhen University Guangdong 518060 P.R. China) X Xuan Wang Z Zhuangqiang Gao (Marshall Laboratory of Biomedical Engineering, Precision Medicine and Health Research Institute, Shenzhen Key Laboratory for Nano-Biosensing Technology, Guangdong Key Laboratory of Biomedical Measurements and Ultrasound Imaging, School of Biomedical Engineering, Shenzhen University Medical School) H Haifeng Dong (Marshall Laboratory of Biomedical Engineering, Precision Medicine and Health Research Institute, Shenzhen Key Laboratory for Nano-Biosensing Technology, Guangdong Key Laboratory of Biomedical Measurements and Ultrasound Imaging, School of Biomedical Engineering, Shenzhen University Medical School)

Abstract

Abstract Although nanozyme‐mediated disruption of mitochondrial homeostasis holds significant therapeutic potential, precise spatiotemporal regulation using single‐function catalysts remains a major challenge. To overcome this limitation, we developed a triphenylphosphine‐functionalized Pd@PtIr nanozyme by epitaxially depositing a Pt–Ir (1:1) alloy shell onto Pd nanocube cores with atomic‐level precision. This rationally engineered metal‐center architecture generates a synergistic catalytic interface that not only enhances peroxidase‐like activity—validated by density functional theory (DFT)—but also endows the nanozyme with intrinsic NADH oxidase and glutathione peroxidase‐like functionalities within a single platform. Upon 808 nm near‐infrared (NIR) irradiation, the nanozyme triggers a cascade of enzyme‐mimetic redox reactions that jointly deplete mitochondrial glutathione (GSH) and elevate reactive oxygen species (ROS) levels, while NADH oxidation concurrently disrupts ATP biosynthesis. These concerted effects synergistically impair mitochondrial redox homeostasis and energy metabolism in tumor cells. To further potentiate therapeutic efficacy, we combined the nanozyme with antisense oligonucleotide‐mediated silencing of ASncmtRNA, resulting in a pronounced 89.1% tumor regression in an orthotopic breast cancer model. This integrated approach—combining atomic‐precision catalyst design, multifunctional enzymatic activity, and gene‐silencing therapy—presents a transformative paradigm for organelle‐targeted precision nanotherapeutics in oncology.

Article Details

Volume / Issue Vol. 65, Issue 9
Published February 23, 2026
ISSN 1433-7851
Publisher Wiley

Journal Info

Angewandte Chemie International Edition

Wiley

ISSN: 1433-7851 Physical Sciences

Authors (13)

Y

Yufan Zhang

Key Laboratory of Photochemistry, Research/Education Center for Excellence in Molecular Sciences, Institute of Chemistry, Chinese Academy of Sciences

S

Shuangshuang Yang

Q

Qin Xiang

Marshall Laboratory of Biomedical Engineering, Precision Medicine and Health Research Institute, Shenzhen Key Laboratory for Nano-Biosensing Technology, Guangdong Key Laboratory of Biomedical Measurements and Ultrasound Imaging, School of Biomedical Engineering, Shenzhen University Medical School

J

Jinkun Huang

Marshall Laboratory of Biomedical Engineering, Precision Medicine and Health Research Institute, Shenzhen Key Laboratory for Nano-Biosensing Technology, Guangdong Key Laboratory of Biomedical Measurements and Ultrasound Imaging, School of Biomedical Engineering, Shenzhen University Medical School

Y

Yongfeng Tan

Marshall Laboratory of Biomedical Engineering, Research Center for Biosensor and Nanotheranostic, School of Biomedical Engineering, Health Science Center Shenzhen University Guangdong 518060 P.R. China

X

Xiang Peng

Department of Neurobiology, School of Basic Medicine, Tongji Medical College, Huazhong University of Science and Technology

Y

Youming Feng

State Key Laboratory of Analytical Chemistry for Life Science, School of Chemistry and Chemical Engineering Nanjing University Nanjing 210023 P.R. China

R

Ran Chang

J

Jinze Li

CAS Key Lab of Bio-Medical Diagnostics

Y

Yaru Cheng

Marshall Laboratory of Biomedical Engineering, Research Center for Biosensor and Nanotheranostic, School of Biomedical Engineering, Health Science Center Shenzhen University Guangdong 518060 P.R. China

X

Xuan Wang

Z

Zhuangqiang Gao

Marshall Laboratory of Biomedical Engineering, Precision Medicine and Health Research Institute, Shenzhen Key Laboratory for Nano-Biosensing Technology, Guangdong Key Laboratory of Biomedical Measurements and Ultrasound Imaging, School of Biomedical Engineering, Shenzhen University Medical School

H

Haifeng Dong

Marshall Laboratory of Biomedical Engineering, Precision Medicine and Health Research Institute, Shenzhen Key Laboratory for Nano-Biosensing Technology, Guangdong Key Laboratory of Biomedical Measurements and Ultrasound Imaging, School of Biomedical Engineering, Shenzhen University Medical School