Aqueous Upcycling of Polyethylene Furanoate From Mixed Plastic Feeds Into Metal‐Organic Frameworks

T Tristan T. Y. Tan (Laboratory of Green Porous Materials Institute of Materials Research and Engineering (IMRE), Agency for Science, Technology and Research (A*STAR) Singapore Republic of Singapore) J Jiawei Huang C Clemen J. G. Goh (Laboratory of Green Porous Materials Institute of Materials Research and Engineering (IMRE), Agency for Science, Technology and Research (A*STAR) Singapore Republic of Singapore) W Wei Wei Loh (Institute of Materials Research and Engineering (IMRE), Agency for Science, Technology and Research (A*STAR), Fusionopolis Way, Innovis #08-03, Singapore 138634, Republic of Singapore) H Hencong Huang (Institute For Integrated Cell‐Material Sciences, Kyoto University Institute For Advanced Study Kyoto University, Yoshida Ushinomiya‐Cho Sakyo‐ku Kyoto Japan) K Ken‐ichi Otake (Laboratory of Green Porous Materials Institute of Materials Research and Engineering (IMRE), Agency for Science, Technology and Research (A*STAR) Singapore Republic of Singapore) Q Qianyu Lin (Institute of Materials Research and Engineering (IMRE), Agency for Science, Technology andResearch (A*STAR), 2 Fusionopolis Way, Innovis #08-03, Singapore 138634, Singapore) W Wenyi Zeng (Laboratory of Green Porous Materials Institute of Materials Research and Engineering (IMRE), Agency for Science, Technology and Research (A*STAR) Singapore Republic of Singapore) Y Yinqiao Wang (School of Physics) D Derek Yiren Ong (JEOL Asia Pte. Ltd., 2 Corporation Road #01-12, Corporation Place Lobby A, Singapore 618494, Singapore) S Susumu Kitagawa (Institute for Integrated Cell-Material Sciences, Kyoto University Institute for Advanced Study, Kyoto University, Yoshida Ushinomiya-cho, Sakyo-ku, Kyoto 606-8501, Japan) K Kai Lan J Jason Y. C. Lim (Institute of Materials Research and Engineering (IMRE), Agency for Science, Technology and Research (A*STAR), Fusionopolis Way, Innovis #08-03, Singapore 138634, Republic of Singapore)

Abstract

ABSTRACT Mixed and contaminated plastic waste is the dominant obstacle to plastics' circularity because most recycling or upcycling technologies require clean, pre‐sorted feedstocks. Here, we demonstrate a sorting‐free upcycling method with purification embedded in upcycling. Polyethylene furanoate (PEF), an emerging biomass‐derived polyester, is converted in water into the valuable metal‐organic framework (MOF) MIL‐160 in high yield. This method remains effective when using unsorted polymer mixtures, including mixtures containing competing polyesters such as polyethylene terephthalate (PET) and polylactic acid (PLA), yielding a pure MOF with no loss in sorption performance. To address the MOF's own end‐of‐life, we demonstrate the ease of recovering 2,5‐furan‐dicarboxylic acid (FDCA) from MIL‐160 for recycling and redeployment to produce other MOFs such as CAU‐28. This connects plastic upcycling to MOF end‐of‐life management, showing that the upcycled product is not a dead‐end material but a reversible reservoir of FDCA that can be recovered and recirculated. Life cycle assessment showed that producing MIL‐160 from mixed PET/PEF plastic feedstock results in a 31% reduction in life‐cycle global warming potential compared to using biomass directly. Additionally, techno‐economic analysis supported the economic feasibility of producing MIL‐160 from mixed PET/PEF. Valorizing PEF into MOFs with diverse applications offers viable end‐of‐life solutions for these bioplastics.

Article Details

Volume / Issue Vol. 65, Issue 21
Published May 18, 2026
ISSN 1433-7851
Publisher Wiley

Journal Info

Angewandte Chemie International Edition

Wiley

ISSN: 1433-7851 Physical Sciences

Authors (13)

T

Tristan T. Y. Tan

Laboratory of Green Porous Materials Institute of Materials Research and Engineering (IMRE), Agency for Science, Technology and Research (A*STAR) Singapore Republic of Singapore

J

Jiawei Huang

C

Clemen J. G. Goh

Laboratory of Green Porous Materials Institute of Materials Research and Engineering (IMRE), Agency for Science, Technology and Research (A*STAR) Singapore Republic of Singapore

W

Wei Wei Loh

Institute of Materials Research and Engineering (IMRE), Agency for Science, Technology and Research (A*STAR), Fusionopolis Way, Innovis #08-03, Singapore 138634, Republic of Singapore

H

Hencong Huang

Institute For Integrated Cell‐Material Sciences, Kyoto University Institute For Advanced Study Kyoto University, Yoshida Ushinomiya‐Cho Sakyo‐ku Kyoto Japan

K

Ken‐ichi Otake

Laboratory of Green Porous Materials Institute of Materials Research and Engineering (IMRE), Agency for Science, Technology and Research (A*STAR) Singapore Republic of Singapore

Q

Qianyu Lin

Institute of Materials Research and Engineering (IMRE), Agency for Science, Technology andResearch (A*STAR), 2 Fusionopolis Way, Innovis #08-03, Singapore 138634, Singapore

W

Wenyi Zeng

Laboratory of Green Porous Materials Institute of Materials Research and Engineering (IMRE), Agency for Science, Technology and Research (A*STAR) Singapore Republic of Singapore

Y

Yinqiao Wang

School of Physics

D

Derek Yiren Ong

JEOL Asia Pte. Ltd., 2 Corporation Road #01-12, Corporation Place Lobby A, Singapore 618494, Singapore

S

Susumu Kitagawa

Institute for Integrated Cell-Material Sciences, Kyoto University Institute for Advanced Study, Kyoto University, Yoshida Ushinomiya-cho, Sakyo-ku, Kyoto 606-8501, Japan

K

Kai Lan

J

Jason Y. C. Lim

Institute of Materials Research and Engineering (IMRE), Agency for Science, Technology and Research (A*STAR), Fusionopolis Way, Innovis #08-03, Singapore 138634, Republic of Singapore