Apoptosis‐Amplified Intracellular Paclitaxel Nanoparticle Formation Enhances Microtubule Aggregation and PANoptosis

X Xiaoyang Liu (Department of Chemical and Biological Engineering) X Xianbao Sun (State Key Laboratory of Digital Medical Engineering, School of Biological Science and Medical Engineering) Y Yu Ma Q Qiaochu Jiang (State Key Laboratory of Digital Medical Engineering, School of Biological Science and Medical Engineering) Y Yun Yin H Hai‐Dong Xu (State Key Laboratory of Digital Medical Engineering School of Biological Science and Medical Engineering Southeast University Nanjing China) X Xiaotong Cheng (State Key Laboratory of Digital Medical Engineering, School of Biological Science and Medical Engineering) Y Yang Yang Y Yinghuan Li (Key Laboratory of Luminescence Analysis and Molecular Sensing, Ministry of Education, College of Chemistry and Chemical Engineering Southwest University Chongqing 400715 China) H Hongzhe Yan (State Key Laboratory of Digital Medical Engineering, School of Biological Science and Medical Engineering Southeast University 2 Southeast University Road Nanjing 211189 China) X Xinping Zhang X Xinwang Yu (State Key Laboratory of Digital Medical Engineering, School of Biological Science and Medical Engineering Southeast University 2 Southeast University Road Nanjing 211189 China) W Wenjun Zhan (State Key Laboratory of Digital Medical Engineering, School of Biological Science and Medical Engineering) F Fu‐Gen Wu (State Key Laboratory of Digital Medical Engineering, School of Biological Science and Medical Engineering Southeast University 2 Southeast University Road Nanjing 211189 China) X Xiaofeng Wu (Materials Innovation Factory, Department of Chemistry) Y Ying Zhuo G Gaolin Liang (State Key Laboratory of Digital Medical Engineering, School of Biological Science and Medical Engineering)

Abstract

Abstract The clinical efficacy of paclitaxel is limited by systemic toxicity at high doses and poor cellular uptake of nanoformulations. Intracellular paclitaxel nanostructure formation is a promising strategy, yet further enhancing its anticancer effect remains challenging. Herein, we propose a strategy of intracellular apoptosis‐amplified paclitaxel nanoparticle formation by rationally designing a caspase‐3‐responsive peptide‐paclitaxel conjugate Ac‐Asp‐Glu‐Val‐Asp‐Cys(StBu)‐Lys(paclitaxel)‐CBT (Ac‐DEVDC(StBu)K(PTX)‐CBT). Upon intracellular glutathione reduction and caspase‐3 cleavage, Ac‐DEVDC(StBu)K(PTX)‐CBT undergoes a CBT‐Cys click reaction and subsequent self‐assembly into paclitaxel nanoparticles. These nanoparticles aggregate microtubules and promote apoptosis, thereby activating more caspase‐3 to drive further nanoparticle formation, creating an amplification loop for enhancing therapeutic outcome. In vitro, Ac‐DEVDC(StBu)K(PTX)‐CBT remarkably inhibited cell cycle, downregulated phosphorylated YAP‐1 level by ∼48%, and induced ZBP‐1/AIM2‐based PANoptosis. Furthermore, in orthotopic tumor models, Ac‐DEVDC(StBu)K(PTX)‐CBT significantly increased caspase‐3 expression compared to free paclitaxel treatment and markedly prolonged survival via cytoskeleton disruption. This strategy holds high promise for enhanced tumor treatment in the clinic.

Article Details

Volume / Issue Vol. 65, Issue 6
Published February 02, 2026
ISSN 1433-7851
Publisher Wiley

Journal Info

Angewandte Chemie International Edition

Wiley

ISSN: 1433-7851 Physical Sciences

Authors (17)

X

Xiaoyang Liu

Department of Chemical and Biological Engineering

X

Xianbao Sun

State Key Laboratory of Digital Medical Engineering, School of Biological Science and Medical Engineering

Y

Yu Ma

Q

Qiaochu Jiang

State Key Laboratory of Digital Medical Engineering, School of Biological Science and Medical Engineering

Y

Yun Yin

H

Hai‐Dong Xu

State Key Laboratory of Digital Medical Engineering School of Biological Science and Medical Engineering Southeast University Nanjing China

X

Xiaotong Cheng

State Key Laboratory of Digital Medical Engineering, School of Biological Science and Medical Engineering

Y

Yang Yang

Y

Yinghuan Li

Key Laboratory of Luminescence Analysis and Molecular Sensing, Ministry of Education, College of Chemistry and Chemical Engineering Southwest University Chongqing 400715 China

H

Hongzhe Yan

State Key Laboratory of Digital Medical Engineering, School of Biological Science and Medical Engineering Southeast University 2 Southeast University Road Nanjing 211189 China

X

Xinping Zhang

X

Xinwang Yu

State Key Laboratory of Digital Medical Engineering, School of Biological Science and Medical Engineering Southeast University 2 Southeast University Road Nanjing 211189 China

W

Wenjun Zhan

State Key Laboratory of Digital Medical Engineering, School of Biological Science and Medical Engineering

F

Fu‐Gen Wu

State Key Laboratory of Digital Medical Engineering, School of Biological Science and Medical Engineering Southeast University 2 Southeast University Road Nanjing 211189 China

X

Xiaofeng Wu

Materials Innovation Factory, Department of Chemistry

Y

Ying Zhuo

G

Gaolin Liang

State Key Laboratory of Digital Medical Engineering, School of Biological Science and Medical Engineering