Achieving Near‐Infrared Organic Room‐Temperature Phosphorescence for High‐Resolution Immune Response Monitoring and Bioimaging

Y Yeyun Zhao X Xianbin Ma (School of Medical Technology Beijing Institute of Technology Beijing 100081 P.R. China) S Shisheng Cui (Beijing Key Laboratory of Construction Tailorable Advanced Functional Materials and Green Applications School of Materials Science and Engineering Beijing Institute of Technology Beijing 100081 P.R. China) J Jiamin Qu (Beijing Key Laboratory of Construction Tailorable Advanced Functional Materials and Green Applications School of Materials Science and Engineering Beijing Institute of Technology Beijing 100081 P.R. China) Y Yuqi Wen K Kai Zhang G Gengchen Li Y Yongfeng Zhang X Xiaoyuan Huang B Baicheng Mei (Department of Materials Science and Engineering, University of Illinois 1 , Urbana, Illinois 61801,) T Tao Wang P Peng Sun (State Key Laboratory of NBC Protection for Civilian) J Jianbing Shi B Bin Tong H Hai‐Yan Xie (School of Pharmaceutical Sciences Peking University Beijing 100191 P.R. China) Z Zitong Liu (State Key Laboratory of Natural Product Chemistry, Key Laboratory of Special Function Materials and Structure Design (MOE), College of Chemistry and Chemical Engineering) Z Zhengxu Cai Y Yuping Dong

Abstract

Abstract Organic near‐infrared (NIR) room‐temperature phosphorescent (RTP) materials hold great potential for bioimaging due to their ability to eliminate background noise and tissue autofluorescence. Here, we synthesized octa‐ring fused RTP molecules (TPP‐BN and TPP‐BF) with B─N coordination bonds via a two‐step reaction, enabling NIR phosphorescent emission at 819 nm and a 28.6 ms lifetime. Using PMMA‐b‐PEG as host and surfactant to stabilize the RTP molecules, we fabricated PMMA‐b‐PEG based nanoparticles (PNPs) with five‐fold brighter afterglow than conventional F127‐based methods (FNPs). We further developed a granzyme B (GrB)‐responsive nanoprobe (Q‐BFNP) that achieves specific and quantitative detection. In vivo studies demonstrated their ability to monitor and distinguish tumor immune response with the signal‐to‐background ratio (SBR) as high as 216.4. This study provides a new method for constructing NIR organic RTP probes and advances applications of RTP materials in real‐time, high‐contrast bioimaging and tumor immune monitoring.

Article Details

Volume / Issue Vol. 64, Issue 47
Published November 17, 2025
ISSN 1433-7851
Publisher Wiley

Journal Info

Angewandte Chemie International Edition

Wiley

ISSN: 1433-7851 Physical Sciences

Authors (18)

Y

Yeyun Zhao

X

Xianbin Ma

School of Medical Technology Beijing Institute of Technology Beijing 100081 P.R. China

S

Shisheng Cui

Beijing Key Laboratory of Construction Tailorable Advanced Functional Materials and Green Applications School of Materials Science and Engineering Beijing Institute of Technology Beijing 100081 P.R. China

J

Jiamin Qu

Beijing Key Laboratory of Construction Tailorable Advanced Functional Materials and Green Applications School of Materials Science and Engineering Beijing Institute of Technology Beijing 100081 P.R. China

Y

Yuqi Wen

K

Kai Zhang

G

Gengchen Li

Y

Yongfeng Zhang

X

Xiaoyuan Huang

B

Baicheng Mei

Department of Materials Science and Engineering, University of Illinois 1 , Urbana, Illinois 61801,

T

Tao Wang

P

Peng Sun

State Key Laboratory of NBC Protection for Civilian

J

Jianbing Shi

B

Bin Tong

H

Hai‐Yan Xie

School of Pharmaceutical Sciences Peking University Beijing 100191 P.R. China

Z

Zitong Liu

State Key Laboratory of Natural Product Chemistry, Key Laboratory of Special Function Materials and Structure Design (MOE), College of Chemistry and Chemical Engineering

Z

Zhengxu Cai

Y

Yuping Dong