A Single‐Molecule Liposome Assay for Membrane Permeabilization

K Krzysztof M. Bąk (EaStCHEM School of Chemistry University of Edinburgh Joseph Black Building, David Brewster Rd Edinburgh EH9 3FJ UK) D Daniel C. Edwards (EaStCHEM School of Chemistry University of Edinburgh Joseph Black Building, David Brewster Rd Edinburgh EH9 3FJ UK) D Dylan George (EaStCHEM School of Chemistry University of Edinburgh Joseph Black Building, David Brewster Rd Edinburgh EH9 3FJ UK) B Bhanu Singh (EaStCHEM School of Chemistry University of Edinburgh Joseph Black Building, David Brewster Rd Edinburgh EH9 3FJ UK) R Ryan Ferguson (EaStCHEM School of Chemistry University of Edinburgh Joseph Black Building, David Brewster Rd Edinburgh EH9 3FJ UK) T Tianxiao Zhao (EaStCHEM School of Chemistry University of Edinburgh Joseph Black Building, David Brewster Rd Edinburgh EH9 3FJ UK) K Kristin Piché (StressMarq Biosciences Inc., 118-1537 Hillside Avenue, Victoria BC V8T 2C1, British Columbia) A Ariel Louwrier S Scott L. Cockroft (EaStCHEM School of Chemistry, University of Edinburgh, Joseph Black Building, David Brewster Rd, Edinburgh, EH9 3FJ, United Kingdom) M Mathew H. Horrocks (EaStCHEM School of Chemistry University of Edinburgh Joseph Black Building, David Brewster Rd Edinburgh EH9 3FJ UK)

Abstract

Abstract Cell membrane disruption is associated with numerous diseases and underlies the activity of various antimicrobial agents. The rapid screening of compounds capable of disrupting or permeabilizing biological membranes is essential to the search for new therapeutic drugs. Here, we present a single‐molecule confocal microscopy assay integrated with fast‐flow microfluidics to study membrane permeabilization in large unilamellar vesicles (LUVs) containing as few as seven dye molecules. This assay eliminates the need for liposome immobilization and achieves detection rates in the range of 1000 vesicles per minute, offering unparalleled sensitivity and detection limits as low as 135 pM, corresponding to just eight permeabilizing molecules per vesicle for active compounds such as ionomycin. It provides a robust platform for investigating membrane‐disrupting agents, including those with antimicrobial properties or implicated in neurodegenerative diseases.

Article Details

Volume / Issue Vol. 64, Issue 26
Published June 24, 2025
ISSN 1433-7851
Publisher Wiley

Journal Info

Angewandte Chemie International Edition

Wiley

ISSN: 1433-7851 Physical Sciences

Authors (10)

K

Krzysztof M. Bąk

EaStCHEM School of Chemistry University of Edinburgh Joseph Black Building, David Brewster Rd Edinburgh EH9 3FJ UK

D

Daniel C. Edwards

EaStCHEM School of Chemistry University of Edinburgh Joseph Black Building, David Brewster Rd Edinburgh EH9 3FJ UK

D

Dylan George

EaStCHEM School of Chemistry University of Edinburgh Joseph Black Building, David Brewster Rd Edinburgh EH9 3FJ UK

B

Bhanu Singh

EaStCHEM School of Chemistry University of Edinburgh Joseph Black Building, David Brewster Rd Edinburgh EH9 3FJ UK

R

Ryan Ferguson

EaStCHEM School of Chemistry University of Edinburgh Joseph Black Building, David Brewster Rd Edinburgh EH9 3FJ UK

T

Tianxiao Zhao

EaStCHEM School of Chemistry University of Edinburgh Joseph Black Building, David Brewster Rd Edinburgh EH9 3FJ UK

K

Kristin Piché

StressMarq Biosciences Inc., 118-1537 Hillside Avenue, Victoria BC V8T 2C1, British Columbia

A

Ariel Louwrier

S

Scott L. Cockroft

EaStCHEM School of Chemistry, University of Edinburgh, Joseph Black Building, David Brewster Rd, Edinburgh, EH9 3FJ, United Kingdom

M

Mathew H. Horrocks

EaStCHEM School of Chemistry University of Edinburgh Joseph Black Building, David Brewster Rd Edinburgh EH9 3FJ UK