A planar-sheet nongraphitic zero-bandgap sp <sup>2</sup> carbon phase made by the low-temperature reaction of γ-graphyne

A Ali E. Aliev (Alan G. MacDiarmid NanoTech Institute, University of Texas at Dallas) Y Yongzhe Guo (School of Civil Engineering, Wuhan University) A Alexandre F. Fonseca (Universidade Estadual de Campinas, Instituto de Física Gleb Wataghin, Departamento de Física Aplicada) J Joselito M. Razal (Institute for Frontier Materials, Deakin University) Z Zhong Wang (Alan G. MacDiarmid NanoTech Institute, University of Texas at Dallas) D Douglas S. Galvão (Universidade Estadual de Campinas, Instituto de Física Gleb Wataghin, Departamento de Física Aplicada) C Claire M. Bolding (Department of Macromolecular Science and Engineering, Case Western Reserve University) N Nathaniel E. Chapman-Wilson (Department of Macromolecular Science and Engineering, Case Western Reserve University) V Victor G. Desyatkin (Department of Macromolecular Science and Engineering, Case Western Reserve University) J Johannes E. Leisen (School of Chemistry and Biochemistry, Georgia Institute of Technology) L Luiz A. Ribeiro Junior (Institute of Physics and Computational Materials Laboratory, Institute of Physics, University of Brasília) G Guilherme B. Kanegae (Universidade Estadual de Campinas, Instituto de Física Gleb Wataghin, Departamento de Física Aplicada) P Peter Lynch (Institute for Frontier Materials, Deakin University) J Jizhen Zhang (Institute for Frontier Materials, Deakin University) M Mia A. Judicpa (Institute for Frontier Materials, Deakin University) A Aaron M. Parra (Alan G. MacDiarmid NanoTech Institute, University of Texas at Dallas) M Mengmeng Zhang (Breast Center) E Enlai Gao (School of Civil Engineering, Wuhan University) L Lifang Hu (Materials Science and Engineering, University of Texas at Dallas) V Valentin O. Rodionov (Department of Macromolecular Science and Engineering, Case Western Reserve University) R Ray H. Baughman (Alan G. MacDiarmid NanoTech Institute, University of Texas at Dallas)

Abstract

The highest sheet symmetry form of graphyne, with one triple bond between each neighboring hexagon in graphene, irreversibly transforms exothermically at ambient pressure and low temperatures into a nongraphitic, planar-sheet, zero-bandgap phase consisting of intrasheet-bonded sp 2 carbons. The synthesis of this sp 2 carbon phase is demonstrated, and other carbon phases are described for possible future synthesis from graphyne without breaking graphyne bonds. While measurements and theory indicate that the reacting graphyne becomes nonplanar because of sheet wrinkling produced by dimensional mismatch between reacted and nonreacted sheet regions, sheet planarity is regained when the reaction is complete. Although the observed elimination of triple bonds to make parallel planar sp 2 carbon sheets likely requires ordered transformation within each sheet, diffraction data for reacted multisheet stacks indicate that the relative lateral positions of neighboring sheets are disordered, as predicted, since no crystalline diffraction peak (other than for the intersheet spacing) is observed.

Article Details

Volume / Issue Vol. 122, Issue 5
Published February 04, 2025
ISSN 0027-8424
Publisher National Academy of Sciences

Authors (21)

A

Ali E. Aliev

Alan G. MacDiarmid NanoTech Institute, University of Texas at Dallas

Y

Yongzhe Guo

School of Civil Engineering, Wuhan University

A

Alexandre F. Fonseca

Universidade Estadual de Campinas, Instituto de Física Gleb Wataghin, Departamento de Física Aplicada

J

Joselito M. Razal

Institute for Frontier Materials, Deakin University

Z

Zhong Wang

Alan G. MacDiarmid NanoTech Institute, University of Texas at Dallas

D

Douglas S. Galvão

Universidade Estadual de Campinas, Instituto de Física Gleb Wataghin, Departamento de Física Aplicada

C

Claire M. Bolding

Department of Macromolecular Science and Engineering, Case Western Reserve University

N

Nathaniel E. Chapman-Wilson

Department of Macromolecular Science and Engineering, Case Western Reserve University

V

Victor G. Desyatkin

Department of Macromolecular Science and Engineering, Case Western Reserve University

J

Johannes E. Leisen

School of Chemistry and Biochemistry, Georgia Institute of Technology

L

Luiz A. Ribeiro Junior

Institute of Physics and Computational Materials Laboratory, Institute of Physics, University of Brasília

G

Guilherme B. Kanegae

Universidade Estadual de Campinas, Instituto de Física Gleb Wataghin, Departamento de Física Aplicada

P

Peter Lynch

Institute for Frontier Materials, Deakin University

J

Jizhen Zhang

Institute for Frontier Materials, Deakin University

M

Mia A. Judicpa

Institute for Frontier Materials, Deakin University

A

Aaron M. Parra

Alan G. MacDiarmid NanoTech Institute, University of Texas at Dallas

M

Mengmeng Zhang

Breast Center

E

Enlai Gao

School of Civil Engineering, Wuhan University

L

Lifang Hu

Materials Science and Engineering, University of Texas at Dallas

V

Valentin O. Rodionov

Department of Macromolecular Science and Engineering, Case Western Reserve University

R

Ray H. Baughman

Alan G. MacDiarmid NanoTech Institute, University of Texas at Dallas