A Modular Platform for Enhanced Drug Delivery to Glioblastoma Using Targeted Multidomain Protein Assemblies

A Andrew L. Wang (Department of Chemical and Biomolecular Engineering New York University Tandon School of Engineering 6 MetroTech Center Brooklyn NY 11201 USA) A Aparajita Bhattacharya (Department of Chemical and Biomolecular Engineering New York University Tandon School of Engineering 6 MetroTech Center Brooklyn NY 11201 USA) F Frances Lee (Department of Chemical and Biomolecular Engineering New York University Tandon School of Engineering 6 MetroTech Center Brooklyn NY 11201 USA) O Orin Mishkit (Department of Radiology Bernard &amp; Irene Schwartz Center for Biomedical Imaging and Center for Advanced Imaging Innovation and Research New York University Grossman School of Medicine 550 1<sup>st</sup> Avenue New York NY 10016 USA) L Lucas Morales (Department of Chemical and Biomolecular Engineering New York University Tandon School of Engineering 6 MetroTech Center Brooklyn NY 11201 USA) J James A. Tranos (Department of Radiology Bernard &amp; Irene Schwartz Center for Biomedical Imaging and Center for Advanced Imaging Innovation and Research New York University Grossman School of Medicine 550 1<sup>st</sup> Avenue New York NY 10016 USA) H Heather Mao (Department of Chemical and Biomolecular Engineering New York University Tandon School of Engineering 6 MetroTech Center Brooklyn NY 11201 USA) N Neha Rahman (Department of Radiology Bernard &amp; Irene Schwartz Center for Biomedical Imaging and Center for Advanced Imaging Innovation and Research New York University Grossman School of Medicine 550 1<sup>st</sup> Avenue New York NY 10016 USA) J Joshua D. Frenster (Department of Neurosurgery New York University Grossman School of Medicine 550 1<sup>st</sup> Avenue New York NY 10016 USA) N Niklas Ravn‐Boess (Department of Neurosurgery New York University Grossman School of Medicine 550 1<sup>st</sup> Avenue New York NY 10016 USA) N Naomi Crook (Department of Chemical and Biomolecular Engineering New York University Tandon School of Engineering 6 MetroTech Center Brooklyn NY 11201 USA) Y Youssef Z. Wadghiri (Department of Radiology Bernard &amp; Irene Schwartz Center for Biomedical Imaging and Center for Advanced Imaging Innovation and Research New York University Grossman School of Medicine 550 1<sup>st</sup> Avenue New York NY 10016 USA) D Dimitris G. Placantonakis (Perlmutter Cancer Center, New York University Langone Health) J Jin Kim Montclare (Department of Chemical and Biomolecular Engineering New York University Tandon School of Engineering 6 MetroTech Center Brooklyn NY 11201 USA)

Abstract

Abstract Protein‐based nanocarriers bear highly desirable properties such as biodegradability and the ability to facilitate passage through biological barriers such as the blood–brain‐barrier. Using modular protein engineering, we develop a strategy for iteratively improving the delivery efficacy of hydrophobic small molecules for the treatment of glioblastoma multiforme (GBM). By increasing the multiplicity m of the coiled‐coil and RGD peptide targeting regions from 1 to 2, we can increase both the hydrodynamic micellar size and drug loading capacity of the targeted multidomain protein assembly (TMPA) relative to its predecessor thermoresponsive assembled protein (TRAP). An upper limit of m is likely determined by steric interactions. TMPA shows a 1.7‐fold increase in doxorubicin (Dox) encapsulation compared to TRAP and demonstrates a 1.3‐fold improvement in uptake by U87 human GBM cells. Near‐infrared (NIR) dye‐labelled TMPA (NIR‐TMPA) is intravenously administered to mice orthotopically implanted with GBM cells and to control mice. Pharmacokinetic analysis using a 2‐compartment pharmacokinetic model reveals a significantly prolonged distribution‐phase (short‐phase) half‐life in tumor‐bearing mice compared to control, while the elimination‐phase (slow‐phase) half‐life remains comparable between groups. This suggests altered early‐phase kinetics likely due to tumor‐associated sequestration or retention. The resulting increased area under the concentration‐time curve (AUC) in tumor‐bearing mice supports enhanced accumulation or slower clearance. Ex vivo fluorescence imaging of organs and 3D reconstructions of whole mouse heads further corroboratesa preferential localization of NIR‐TMPA in tumor regions. These findings highlight the potential of TMPA and its future derivatives for targeted GBM therapy.

Article Details

Volume / Issue Vol. 64, Issue 37
Published September 08, 2025
ISSN 1433-7851
Publisher Wiley

Journal Info

Angewandte Chemie International Edition

Wiley

ISSN: 1433-7851 Physical Sciences

Authors (14)

A

Andrew L. Wang

Department of Chemical and Biomolecular Engineering New York University Tandon School of Engineering 6 MetroTech Center Brooklyn NY 11201 USA

A

Aparajita Bhattacharya

Department of Chemical and Biomolecular Engineering New York University Tandon School of Engineering 6 MetroTech Center Brooklyn NY 11201 USA

F

Frances Lee

Department of Chemical and Biomolecular Engineering New York University Tandon School of Engineering 6 MetroTech Center Brooklyn NY 11201 USA

O

Orin Mishkit

Department of Radiology Bernard &amp; Irene Schwartz Center for Biomedical Imaging and Center for Advanced Imaging Innovation and Research New York University Grossman School of Medicine 550 1<sup>st</sup> Avenue New York NY 10016 USA

L

Lucas Morales

Department of Chemical and Biomolecular Engineering New York University Tandon School of Engineering 6 MetroTech Center Brooklyn NY 11201 USA

J

James A. Tranos

Department of Radiology Bernard &amp; Irene Schwartz Center for Biomedical Imaging and Center for Advanced Imaging Innovation and Research New York University Grossman School of Medicine 550 1<sup>st</sup> Avenue New York NY 10016 USA

H

Heather Mao

Department of Chemical and Biomolecular Engineering New York University Tandon School of Engineering 6 MetroTech Center Brooklyn NY 11201 USA

N

Neha Rahman

Department of Radiology Bernard &amp; Irene Schwartz Center for Biomedical Imaging and Center for Advanced Imaging Innovation and Research New York University Grossman School of Medicine 550 1<sup>st</sup> Avenue New York NY 10016 USA

J

Joshua D. Frenster

Department of Neurosurgery New York University Grossman School of Medicine 550 1<sup>st</sup> Avenue New York NY 10016 USA

N

Niklas Ravn‐Boess

Department of Neurosurgery New York University Grossman School of Medicine 550 1<sup>st</sup> Avenue New York NY 10016 USA

N

Naomi Crook

Department of Chemical and Biomolecular Engineering New York University Tandon School of Engineering 6 MetroTech Center Brooklyn NY 11201 USA

Y

Youssef Z. Wadghiri

Department of Radiology Bernard &amp; Irene Schwartz Center for Biomedical Imaging and Center for Advanced Imaging Innovation and Research New York University Grossman School of Medicine 550 1<sup>st</sup> Avenue New York NY 10016 USA

D

Dimitris G. Placantonakis

Perlmutter Cancer Center, New York University Langone Health

J

Jin Kim Montclare

Department of Chemical and Biomolecular Engineering New York University Tandon School of Engineering 6 MetroTech Center Brooklyn NY 11201 USA