Zhang, J., García‐López, V., Wu, Y., Fu, S., Chen, Y., Hazrah, A. S., Petkov, P., Hambsch, M., Ni, F., Müller, A., Yang, Y., Riemenschneider, L., Huang, S., Sandee, A. M., Guo, Y., Silva‐Brea, D., Joswig, J., Mannsfeld, S. C. B., Heine, T., Cuniberti, G., Bonn, M., Wang, Z., Feng, X. (2026). On‐Water Surface Synthesis of 2D Conjugated Metal–Organic Framework Films With Controllable Layer Orientation Enabling High‐Performance Chemiresistive Sensing. Advanced Materials. https://doi.org/10.1002/adma.73785